GCMS analysis report for sample AE02334, March 2002

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Library Search Compound Report

‘Data File C:\MSDCHEM\l\DATA\030402\2152.D Vial: 6 Acq On 4 Mar 2002 2:21 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.14 6.02 ug/L 2954760 Naphthalene-d8 13.05

Hit# of 5 Tentative MW MolForm CAS# Qual l Cyclohexas iloxane, dodecamethyl-. . . 444 C12H36O6S16 000540-97-6 91 2 Cyclohexasiloxane, < decamethyl - 444 C12H3606Si6 000540-97-6 91 3 METHYL 2,3-BIS(TRIM] LSILYLOXY. . . 341 C16H27DO4Si2 000000-00-0 38 4 2H-1,4-Benzodiazepi; one, 7-ch. . . 342 C18H19C1N2OSi 055299-24-6 35 Abundance Scan 1330 (15.139 min): 2152.D (-) m/z 73.10 100.00%| 73

5000 341

147 ‘I T T T 45 429 14.80 15.00 15.20 15.40 - 01 117 ■ ■ i ■ 1792%7, 251 281 311 381 rl 1 1 ‘ 1 I m/z 341.00 35.71 m/z-> 50 100 150 200 250 300 350 400 Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc... 73 341

429 5000 14.80 15.00 15*20 15.40 111 m/z 147.10 14.96 147 45 0- ■ ' 1 1 , 117 297 , 267.311 [ • I ‘ 397. ' I • ‘ miz-> 50 166 150 200 250 300 350 400 Abundance #352522; Cyclohexasiloxane, dodecamethyl- 73 TT T T T T 14.80 15.00 15.20 15.40 5000 m/z 342.00 12.30%] 341 429 147 45 117 177 207 237 271 3111 367 397 0 • ‘i I >' • 1 • 1 < • r • Y-r-j-h I"I"ImI"prtpvi TTBT m/z-> 50 100 150 200 250 300 350 400 Abundance#289709: METHYL 2,3-BIS(TRIMETHYLSlLYLOXY)-5-DEUTEROPHEN f ________ M._______ 73 180 ■ i ■ < । ■ I ‘ ‘ * i •. ■ • i • • • ■ i 14.80 15.00 15.20 15.40 m/z 429.10 12.00

5000 341 45

0 ,106 .149 — . V । ■ t f. ,•, | 222 268 ,310, I ........ m/z—> 50 100 150 200 250 300 350 400 14.80 15.00 15.20 15'40 ‘

2152.D 5080302.M Mon Mar 18 08:30:25 2002 Page 5

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