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GCMS analysis report for sample AE02334, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010488–000010512

Folder label: “GCMS X 1/31/02 A 3/4/02

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Scanned page image, NYC-WTC_000010498
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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File C:\MSDCHEM\l\DATA\030402\2152.D Vial: 6 Acq On 4 Mar 2002 2:21 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 4 2,5-Dimethylhexane~2,5-dihy... Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

15.98 0.52 ug/L 278323 Acenaphthene-d10 18.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual -------------------------------------- - ------------------------------------------------- 1 2,5-Dimethylhexane-2,5-dihydrope... 178 C8H18O4 003025-88-5 25 2 Ether, 2-ethylhexyl tert.butyl 186 C12H26O 000000-00-0 10 3 Quinuclidine $$ 1-Azabicyclo [2.2 . . . 111 C7H13N 000100-76-5 9 4 5,9-Dimethyl-3-dedanol 186 C12H260 019550-53-9 9 Abundance Scan 1423 (15.983 min): 2152.D (-) m/z 57.10 100.00% 57 73

5000 111 95 =-mpmmmm

mlz-> 20 0 40 60 s 80 | ,44 34, I L 127 _ 145... 193 207 166 Abundance #82883: 2,5-Dimethylhexane-2,5-dihydroperoxide $$ Hydroper... 120 140 160 180 200 15.60 15.80 16.00 16.20 16.40 m/z 73.10 73.53%

43

69 5000 | » t t > | » » 4 | t 1 > Ci 55 111 15.60 15.80 16.00 16.20 16.40 95 m/z 111.10 46.88%

miz-> 0 i ■ '• ■ i 20 40 +2,—— 127 144 163 178 60 80 100 • i • • • ' 1 1 ■ • ■ i • • ■ ■ i ■ ■ • ■ i ■ ■ 120 140 160 180 200 Abundance #95994: Ether, 2-ethylhexyl tert butyl 57

15.60 15.80 16.00 16.20 16.40 5000 m/z 69.10 34.15%

41 29 71 Ot । rr । T > .87 98 113 129 I ' ■ 1 ' i 1 ■ ‘ ‘ 1 • ‘ 1 ' I ' ‘ 157 171......... ‘ I ' ■ ‘ ' i ‘ ' 1 ' 1 ■ ‘ ‘ I ‘ ‘ " m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #12820: Quinuclidine $$ 1-Azabicyclo[2.2.2]octane $$ 1,4-E... __ ... 42 15.60 15.80 16.00 16.20 16.40 m/z 95.10 31.82%

82 111 5000 96

27 55 69 ° 0 ! I 4 । t d । 'I1trr 1 TTt • i • • • • i • • • • i • ■ • • i • • • • j • • m/z-> 20 40 60 80 100 120 140 160 180 200 15*60 15.80 16.00 16'20 16.40

2152.D 5080302.M Mon Mar 18 08:30:26 2002 Page 6

NYC-WTC_000010498

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