NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\5973N\02FEB01\31134.D Vial: 3
Acq On : 1 Feb 2002 4:24 pm Operator:
Sample : 508 scan Inst : Instrumen
Mise : February 1, 2002 Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator)
Title : 508 scan method
Library : C:\DATABASE\WILEY7N.L
*********************************************************************
Peak Number 10 (E)-5-Methyl-2-methylene-2-... Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
16.25 0.08 ug/L 53092 Acenaphthene-dl0 18.34
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 (E)-5-Methyl-2-methylene-2-hexen... 126 C8H140 000000-00-0 9
2 Palustrol $$ 4aH-Cycloprop[e]azu... 222 C15H260 005986-49-2 9
3 Hydroperoxide, 1-ethylpropyl $$ ... 104 C5H12O2 024254-57-7 9
4 Oxirane, [(1-methylethoxy)methyl]- 116 C6H1202 004016-14-2 9
Abundance Scan 1128 (16.252 min): 31134.D (-) m/ z 43.10 100.00%
43
_AA
57
111
5000
49
73
84
95 1 —A16.00AAAL
16.20 16.40 16.60
0 " I" " I"1 ‘1"1' IH1 ■ i ----- i" "i'" TTl ‘‘|1111111 I''1 ‘ I ■ i'■" i'1" i'1" i" " i■ m/ Z 57.10 68.13%
mfa-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115
Abundance #23067: (E)-5-Methyl-2-methylene-2-hexen-1-ol
43
5000 59 I
f 1 1 i ' ' 1 1 i ' ■
16.00 16.20 16.40 16.60
49
84
m/ z 59.10 56.14%
0 11’23 1’221115 mmmmHHmnIA-
mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115
Abundance #148519: Palustrol $$ 4aH-Cycloprop[e]azulen-4a-ol, decahy...
43
16.00 16.20 16.40 16.60
55
5000 67 111 m/z 111.10 52.43%
83 93
0- ’’I’1111112711—01111—1T 'l""l T’ 11 “111 1 ’1 ' | 1 11 ‘ 11 “ > 1 TTTp-rrrp
mtz.-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115
Abundance #10168: Hydroperoxide, 1 -ethylpropyl $$ 3-Pentyl hydroperoxid
43 16.00 16.20 16.40 16.60
57 m/ z 73.10 31.84%
71
5000
27
104
mfe->
0- '' I' ‘" I' 1|33.... ' r1" r “' i ■ TMT +rr 1111111111011000 07-1111117
20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 16.00 16.20 16.40 16.60
31134.D SCAN508.M Mon Feb 04 08:41:37 2002 Page 12
NYC-WTC_000004086
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