DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\31134.D Vial: 3 Acq On : 1 Feb 2002 4:24 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 101929 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 3 1-amino-2-methyl-4 -isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 45 Abundance Scan 1656 (22.280 min): 31134.D (-) m/z 192.10 100.00% 192

5000

82 96 146 160 22.00 22.20 22.40 22.60

m/z—> 0- 43 I 66 , 120 I**/ 1" I " 11111111'11' i11 ' 11111ITIPTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 -Hl TTT1 m/ Z 96.00 16.74% Abundance #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/z 191.10 14.35%

0 ’ I’’’AAd’’II’A’II’’’I’++’IIE’II’’III’’ I‘**AI‘A*I/*|‘* ' I " ‘ ‘ I ' ' " I ' TTI TT-p-1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z 146.10 13.54%

54 110 30 m/z-> 0 -H " i " " i' I 94 160 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TTIWTTTITTTTWTTTTWTTTOTITTTTT II

Abundance #10191 8:1 -amino-2-methyi-4-isopropyl-thiotriazaphospholin... 159 192 22.00 22.20 22.40 22.60 m/ z 193.10 12.66%

5000

144 177 asianckpamn) 0 " i " ■ ■ i" ■ ■ i ■ “ ' i " ' ■ i ■ " ‘ i ■ “ ' i' " ' i ■ " ‘ r ■ " i' • " i " " i'1" i " m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

31134.D SCAN508.M Mon Feb 04 08:41:38 2002 Page 13

NYC-WTC_000004087

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999