GCMS analysis results for sample AD31670, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31670 including unknown compounds and surrogate recovery data.

NYC-WTC_000050008–000050023

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02JAN17\31670.D Vial: 5 Acq On : 17 Jan 2002 6:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 106574 Phenanthrene-dl0 22.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 72 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 3 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 1,4-Dimethyl-3,5-propanobicyclot... 192 C13H20O 000000-00-0 47 Abundance Scan 1656 (22.280 min): 31670.D (-) m/z 192.05 100.00% 1912

5000 ....... . 82 96 146 160 22.00 22.20 22.40 22.60 44 70 1 ■ |l> u | <41'1 | I m I 1 I n-| | I |T| I I I I I I A 1i i > l'| i11 > | i r , 0 — mpHe — m/z 191.10 15.54% m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/z 193.10 13.75%

iz—> 0 " i ■ ■ • ■ i ■ ■ ■ ■ i ■ ■1 • i' “ ■ i ‘ ■11'1 ‘ ■ i •1 r "' i ‘ ■11 ■ ■ ■ ■ i ■ ■ • । 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 »। • i • +ri ■ ■ IT 1 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192

22.00 22.20 2240 22.60 5000 m/z 146.10 13.68%

88 J 139 152 165 176 , 0 TIOIWIWmITPTITPImTTTIt Wpr. /z—> 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... ............ A Pi 159 192 22.00 22.20 22.40 22.60 m/z 96.00 12.57% 5000

144 177

T T T n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

.1670.D SCAN508.M Tue Jan 22 08:37:23 2002 Page 10

NYC-WTC_000050021

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GCMS analysis results for sample AD31644, Jan 28 2002 · Box DEP Box 28

NYC-WTC_000049990

Laboratory report showing GCMS analysis of sample AD31644 including unknown compounds and surrogate recovery data.

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