GCMS analysis results for sample AD31670, Jan 28 2002

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Library Search Compound Report . , Data File : C:\MSDCHEM\1\5973N\02JAN17\31670.D Vial: 5 Acq’On : 17 Jan 2002 6:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.29 ug/L 205113 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 93 2 Phenanthrene-dlO 188 C14DiO 001517-22-2 90 3 Anthracene-dlO- 188 C14D10 001719-06-8 87 4 Anthracene-D10 188 C14D10 000000-00-0 87 Abundance Scan 1699 (22.771 min): 31670.D (-) m/z 188.20 100.00% 1(18

5000

80 94 44 ! ----- 57 66 132 158 180 I 22.40 22.60 22.80 23.00 23.20 0- —mmpm TI m/z 94.05 18.64% miz-> 40 50 60 70 80 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188 % 5000 . | > . I I | . T 1 T| n t I J—1--I I 1 I I 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.10 16.16% 66 158 0- —PTPT TTTf mmmPppmmmmmpHmp iz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 13.34%

94 160 80 66 0- —]mmmpmp *HHmm T1 n/z-> 40 50 60 70 80 M 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- ‘fT ,4 i PP i i . । r > i ■ । i 188 22.40 22.60 22.80 23.00 23.20 m/z. 189.10 13.13% 5000

66 80 94 160 . 0 111 > > 11 ] > >> i j 11111 >» ‘1 ■ i 1 ■ • ‘I ITT ■ • ■ r > ‘i miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

31670.D SCAN508.M Tue Jan 22 08:37:23 2002 Page 11

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