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GCMS blank analysis results for sample AE00275, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.

NYC-WTC_000051024–000051039

Folder label: “GCMS X 1/7/02 A 1/8/02

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Scanned page image, NYC-WTC_000051037
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\5973N\02JAN08\00275.D Vial: 1 Acq On : 8 Jan 2002 3:24 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.36 ug/L 186927 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 90 2 Anthracene-DlO 188 C14D10 000000-00-0 90 3 Anthracene-dlO- 188 C14D10 001719-06-8 74 4 Phenanthrene-diO 188 C14D10 001517-22-2 74 Abundance Scan 1699 (22.771 min): 00275.D (-) m/z 188.10 100.00% 188 A 5000

80 94 66 132 146 156 22.40 22.60 22.80 23.00 23.20

n/z-> 0 60 70 — 80 . r-—l 1— 90 100 110 120 130 140 150 160 170 180 190 il m/z 94.00 19.08% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/ Z 80.10 16.91%

miz-> 66 0 ----- *PP 60 70 80 90 100 110 120 130 140 150 160 -1, 158

170 .I.. 180 190 Abundance #84498: Anthracene-D10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 189.10 14.78% 80 94

—PP -------------- —l— 66 160 01 miz-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 10.99%

5000

80 94 160 66

n/z-> 0 Lr H 1041—— TT I ■ ‘ "II 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

00275.D SCAN508.M Wed Jan 09 15:11:00 2002 Page 10

NYC-WTC_000051037

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NYC-WTC_000051037Source: NYC Law Department, mirrored locally

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