GCMS analysis results for sample AE00248, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\00248.D Vial: 4 Acq On : 24 Jan 2002 5:27 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

22.77 0.35 ug/L 270267 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 90 2 Anthracene-dlO- 188 C14D10 001719-06-8 87 3 Anthracene-D10 188 C14D10 000000-00-0 83 4 Phenanthrene-diO 188 C14D10 001517-22-2 78 Abundance Scan 1699 (22.771 min): 00248.D (-) m/z 188.15 100.00% 188

5000 — 94 52 66 80 132 146 160 I, 2240 22.60 22.80 23.00 23.20 1110mmmPITTITITT — 4.... p FTi 11. । ■ I ■ |■ i. | m/z 94.10 16.37% m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 fl Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 108

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 184.10 13.96% 158 . nz—> i ■ ■ “ i1 ‘ 66 ■ i1 •1 ■ i ■1 mm‘t1 I'1 "I‘' " 111 “)' “ 'I 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 r-TT

Abundance #84502: Anthracene-d1 fl- 188

2240 22.60 22.80 23.00 23.20 5000 m/z 189.10 12.42%

80 94 160 66 miz-> 40 mmpmp 50 60 70 80 '' I'1' ‘ I'' ‘ ‘ I " '' I'' " I ‘ 90 1(» 110 120 130 140 150 160 170 180 190 ...... Ill........ 104. Abundance #84498: Anthracene-D10 ■I 1 1 > 11 ' ' 1 rl ‘ ' I ' ' ' ’ I ' 188 22.40 22.60 22.80 23.00 23.20 m/z 92.05 10.29%

5000 80 94

niz-> 40 50 60 70 80 66 PPmmmm 1’ 90 100 110 120 130 140 150 160 170 180 190 160 l - 22.40 22.60 22.80 23.00 23.20

00248.D SCAN508.M Fri Jan 25 10:26:11 2002 Page 14

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