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GCMS analysis results for sample AE00167, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050481–000050499

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050497
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\00167.D Vial: 4 ' Acq On : 24 Jan 2002 2:09 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.33 ug/L 262030 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 95 2 Phenanthrene-diO 188 C14D10 001517-22-2 87 3 Anthracene-dlO- 188 C14D10 001719-06-8 87 4 Anthracene-D10 188 C14D10 000000-00-0 58 Abundance Scan 1699 (22.771 min): 00167. D (-) m/z 188.10 100.00% 188

5000

80 94 m 22.40 22.60 22.80 23.00 23.20 43 52 66 - 132 160 —— TIIH m/z 94.10 16.06% nz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 ... ■ । • ■ ■ ■ । { ■ i ' ■ ■ ■ i ■ ' ■ ■ i ■ 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.10 14.88%

niz-> 40 50 60 66 70 80 mmmfmplapm 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 1118

22.40 22.60 22.80 23.00 23.20 5000 m/z 189.15 10.48%

80 94 160

miz-> 40 00 0000 1 1 50 60 70 80 Alteqll—. 90 1(X) 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- ..... .. ............. 158 22.40 22.60 22.80 23.00 23.20 m/z 184.10 9.59%

5000-

66 80 94 160 , |, mITTTT ■■I....,,!..,....... ............. „..H...... .W.... ----- vtz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

0167.D SCAN508.M Fri Jan 25 10:25:48 2002 Page 13

NYC-WTC_000050497

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NYC-WTC_000050497Source: NYC Law Department, mirrored locally

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