Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
NYC-WTC_000050481–000050499Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\00167.D Vial: 4 • Acq On : 24 Jan 2002 2:09 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 11 R.T. EstConc Area Relative to ISTD • R.T. 26.01 0.09 ug/L 67943 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW Mol Form * CAS# Qual 1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 64 2 Cyclic octaatomic sulfur 256 S8 010544-50-0 64 3 N- (2-Hydroxyethyl) -N’ - [2’ - (-meth. . . 255 C10H13N3O3S 000000-00-0 47 4 Sulfur $$ Sulfur, precipitated $... 256 S8 007704-34-9 38 Abundance Scan 1983 (26.013 min): 00167. D (-) m/z 64.00 100.00% 64
5000 128 160 256 96 192
mlz-> 44 ‘ 1 1 1 1 1 ' 1 1 40 60 L 80 i ‘ ■ • 1 i ' 100 120 140 160 180 200 220 240 1t—nmn/0. Iut 260 25.60 25.80 26.00 26.20 26.40 m/z 127.90 46.19% Abundance #195802: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ 8... 64
5000 m 25.60 25.80 ‘26.00 26.20 26.40 m/z 255.80 45.43% — 96 128 160 192 256 34 1,779—7 1 .1 P • ‘ i 1 ■ 224 i ■ ■ • ■ i 1 ■ ■ • i • • • I ■ • niz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195804: Cyclic octaatomic sulfur 64
25.60 25.80 26.00 26.20 26.40 5000 m/z 159.90 44.50%
128 160 256
miz-> 34 1 1 i ■ ■ ■ ■ i 40 60 L7 80 100 96 140 120 ’ 192 ’ 224 160’ 180 200 220 240′260 Abundance #193372: N-(2-Hydroxyethy!)-N’[2’-(-methoxycarbony!)thiop... 64 25.60 25.80 26.00 26.20 26.40 8000 256 m/z 191.80 25.76%
6000 128 160
4000 96 192 221 ■ ‘ i 1 1 ■ ■ i 1 ‘ I ■ 1 1 । i 1 ' 1 1 1 1 ■ ■ i ■ ■ • i ‘ ‘ ‘ 1 I ‘ ' 1 i ‘ ■ 118 miz—> 40 60 80 100 120 140 160 180 200 220 240 260 25.60 25.80 26.00 26.20 26.40
0167.D SCAN508.M Fri Jan 25 10:25:48 2002 Page 14
NYC-WTC_000050498
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000050596
Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050683
Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050645
Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder