GCMS analysis results for sample AD31677, Jan 2002

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Laboratory report for sample AD31677 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050334–000050348

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\31677.D Vial: 2 Acq On : 23 Jan 2002 3:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 26.01 0.29 ug/L 172367 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Sulfur, mol. (CAS) $$ OCTA-... 256 S8(S8) 010544-50-0 95 2 Sulfur, mol. (CAS) $$ OCTA-... 256 S8(S8) 010544-50-0 90 3 Cyclic octaatomic sulfur 256 S8 010544-50-0 90 4 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 87 Abundance Scan 1983 (26.013 min): 31677.D (-) m/z 63.95 100.00% 64

5000 128 160 256 96 192 m 25.60 25.80 26.00 26.20 26.40

nz-> 0- ■ • i ' ■ ■ ■ i 40 60 176,— 80 —— , I... 1 1_________________ * t * * * ' i * 1 1 * i * * 100 120 140 160 180 200 220 240 260 18.8 m/z 127.90 50.20% Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$S8$$ S... 64

5000 128 256 25.60 25.80 26.00 26.20 26.40 96 160 m/z 255.80 44.73% 192 34 48 niz-> 0U 11 I ' 1 1 1 I । ■ ■ i ■ ■ 40 60 80 I j____________ ■ I' ' ■ ■ I ■ 100 120 140 160 180 200 220 240 224 ■ i ■ ■ ■ ■ i ' ■ ■ ■ i ' ■ 4 260 Abundance #195802: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 i 1 ■ ■ ■ i ■ ■ ■ ■ i ■ • ■ ■ i 1 1 ' ■ i • ■ 25.60 25.80 26.00 26.20 26.40 5000 m/z 159.90 44.62%

96 128 160 256 34 0-r ■ ' । 1 1 1 ‘ i ।"i1 'll 76 ■' 1 I 1 ■ ■ ' i ■ 1 ■ 1 i 1 ■ 192 ..... 224 111444114 UT—t I ' ' 1 1 1 ■ /z—> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195804: Cyclic octaatomic sulfur 64 25.60 25.80 26.00 26.20 26.40 m/z 191.80 24.19% 5000

— 96 128 160 256

iz-> 0- 34 40 i ' ■ ' ■ i 60 L79 80 100 120 140 192 1 TTI—m—T . 224 — 160 180 200 220 240 260 25.60 25.80 26.00 26.20 26.40

31677.D SCAN508.M Thu Jan 24 09:57:39 2002 Page 10

NYC-WTC_000050347

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