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GCMS analysis results for sample AE00830, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00830 including surrogate recovery and unknown compounds.

NYC-WTC_000052047–000052068

Folder label: “GCMS X 1/11/02 A 1/31/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C : \MSDCHEM\1\5973N\02JAN31\00830 . D Vial: 3 Acq On : 31 Jan 2002 12:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 26.00 0.06 ug/L 48752 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 91 2 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 91 3 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 38 010544-50-0 91 4 Cyclic octaatomic sulfur 256 S8 010544-50-0 91 Abundance Scan 1982 (26.002 min): 00830. D (-) m/z 64.00 100.00% 64

5000 128 160 96 192 256 44 84 25.60 25.80 26.00 26.20 26.40 0 H II, , , I, , f , I, , - m/z 127.90 33.32% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195803: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64

5000 I ' 1 1 1 I ' 1 1 1 I ’ 1 r 1 I ' 1 1 1 1 1 1 256 25.60 25.80 26.00 26.20 26.40 128 160 m/z 159.90 29.46% 96 192

m/z-> 0- 44 । । । | । ‘ । I I 40 60 1...... 80 I'100 ........ 120 140 I, , , , 160 180 200 '... .. It 220 240 260 Abundance #195802: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 25.60 25.80 26.00 26.20 26.40 5000 m/z 255.80 22.56%

76 96 128 256

m/z-> 0 34 1 ■ i ■ ' 1 1 i 40 60 L79 80 100 120 140 160

160 - 192 224........... | 180 200 220 240 260 Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... i rrri 1 "‘‘IT I"’ ' r11 64 25.60 25.80 26.00 26.20 26.40 m/z 191.80 '18.47% 5000 128 256 96 160 192 34 48 I......... i............. j,............. 224 .......... m/z-> 0 11 1 1 1 1 1 i 40 60 ' 1 ' i ■ ■ 80 100 120 I........... 140 160 180 200 220 240 TTur 260 . .......... 1V 25.60 25.80 26.00 26.20 26.40

10830.D SCAN508.M Fri Feb 01 09:18:33 2002 Page 15

NYC-WTC_000052065

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NYC-WTC_000052065Source: NYC Law Department, mirrored locally

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