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GCMS analysis results for sample AE00838, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052187–000052204

Folder label: “GCMS X 1/11/02 A 1/31/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31 Jan 2002 1:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ************************************************* *** * * ** * * * * ********* Peak Number 11 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

26.01 1.74 ug/L 1260700 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 97 2 Cyclic octaatomic sulfur $$ Sulf... 256 S8 010544-50-0 95 3 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 95 4 Cyclic octaatomic sulfur 256 S8 010544-50-0 94 Abundance Scan 1983 (26.014 min): 00831.D (-) m/z 64.00 100.00% 64

128 160 256 5000 96 192 .... y . 2560 25.80 26.00 26.20 26.40

m/z-> 0- 43 < । I ■ i ' r i +111 1 -trr851 — 1.., ------- 224 —T 80 100 120 140 160 180 200 220 240 260 1 i t ■ ■ ■ i ■ - m/z 127.90 59.25% 40 60 Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64

---- 1 .-r-n । i *) 8 , MT i ■ । , , 5000 128 256 25.60 2580 26.00 26.20 26.40 96 160 m/z 255.80 52.12% 192

m/z-> 34 48 ot ’ ■ ■ । • 1 ■ ■ i I I, 11 I ' ‘ 40 60 80 100 — TT I r 1 11 1 ' 120 140 160 1 180 200 220 240 224 ......."Tr 260 Abundance #195805: Cyclic octaatomic sulfur $$ Sulfur, mol. (S8) $$ ... 64 256 25.60 25.80 26.00 26.20 26.40 128 160 5000 m/z 159.90 48.18% 96 192

224 A m/z-> 0- 34 1 i ' 1 ' 1 I 40 60 - 80 1 i 1 1 1 1T 1 100 120 I, -PPP 140 160 180 200 220 J........... । I 1 | i . » ' | 240 . P 260 Abundance #195806: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 256 25.60 25.80 26.00 26.20 26.40 m/z 191.80 27.03% 160 128 5000

96 192 224 34 I........... - 0 — — ' 1 ■ i ' ' i ' ■ 1 ' 1 1 11 I 'r '■"I...... .. i 1 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 25.60 25.80 26.00 26.20 26.40

30831.D SCAN508.M Fri Feb 01 09:18:44 2002 Page 13

NYC-WTC_000052201

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NYC-WTC_000052201Source: NYC Law Department, mirrored locally

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