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GCMS analysis results for sample AE00830, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00830 including surrogate recovery and unknown compounds.

NYC-WTC_000052047–000052068

Folder label: “GCMS X 1/11/02 A 1/31/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00830.D Vial: 3 Acq On : 31 Jan 2002 12:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ***************************************************************** *** * Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

22.77 0.45 ug/L 352491 Phenanthrene-diO 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-D10 188 C14D10 000000-00-0 86 3 Phenanthrene-diO 188 C14D10 001517-22-2 86 4 Anthracene-dlO- 188 C14D10 001719-06-8 83 Abundance Scan 1699 (22.771 min): 00830.D (-) m/z 188.20 100.00% 188

5000

80 94 ........................ 22.40 22.60 22.80 23.00 23.20 42 52 64 01 -TTT ■ I ■ *............. 1 132 158 । I 1 1 | H 1 i | " I . | l-ri l | I I I I | I I I I | I i i I | i I ‘ i ■ I i | I i m/Z 80.10 19.07% m/z-> 40 50 6070 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-dlO 188

............... ................................... 5000 22.40 22.60 22.80 23.00 23.20 80 94 m/ z 94.10 17.39%

m/z-> 6.6 0- TTITTTTTTTTTTTTT-t-r ontt i1 " ' i'1' ■ i 158 - 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 —l— Abundance #84498: Anthracene-D10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 189.15 16.60% 80 94 160 0 - — mlz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 158 22.40 22.60 22.80 23.00 23.20 m/z 184.10 12.55%

5000

80 94 160 H ...nF... . 66 0 —IPPTTTTI m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

00830.D SCAN508.M Fri Feb 01 09:18:33 2002 Page 14

NYC-WTC_000052064

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NYC-WTC_000052064Source: NYC Law Department, mirrored locally

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