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GCMS analysis results for sample AD31585, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31585 including unknown compounds and surrogate recovery data.

NYC-WTC_000049902–000049915

Folder label: “GCMS X 1/3/02 A 1/17/02

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Scanned page image, NYC-WTC_000049913
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02 JAN17\31585 . D Vial: 1 • Acq On : 17 Jan 2002 2:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ***************************** **************************************** Peak Number 6 DECADEUTEROPHENANTHRENE $$ . . . Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.23 ug/L 107417 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 80 2 Anthracene-dlO- 188 C14D10 001719-06-8 80 3 Phenanthrene-diO 188 C14D10 001517-22-2 80 4 Anthracene-D10 188 C14D10 000000-00-0 64 Abundance Scan 1699 (22.771 min): 31585.D (-) m/z 188.10 100.00% 188

5000 94 80 156 . 22.40 22.60 22.80 23.00 23.20 66 01 118 --H ----- TrT m/z 94.10 21.19% miz-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 .. . . .................. .. 22.40 22.60 22.80 23.00 23.20 80 94 m/z 189.10 16.60% 66 158 — 01 1. TIT Turf —mmm niz-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188 ........... /.......................... **aa,nnnaiT431144/1/4 22.40 22.60 22.80 23.00 23.20 5000 m/z 80.10 13.06%

66 80 *4 160 nz-> 01 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .1801... ........... ....................... Abundance #84499: Phenanthrene-d10 188 22.40 22.60 22.80 23.00 23.20 m/z 184.05 12.97%

5000

80 94 160 66 0 1 r ‘ ■ l1'' mmmmmmmmmm ......ill...... w..„ ----- m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

31585.D SCAN508.M Tue Jan 22 08:36:52 2002 Page 8

NYC-WTC_000049913

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NYC-WTC_000049913Source: NYC Law Department, mirrored locally

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