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GCMS analysis results for sample AD31585, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31585 including unknown compounds and surrogate recovery data.

NYC-WTC_000049902–000049915

Folder label: “GCMS X 1/3/02 A 1/17/02

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NYC 9/11 Public Portal Document Library searen Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN17\31585.D Vial: 1 Acq On : 17 Jan 2002 2:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 8-Benzenesulphonyloxyquinoline Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 33.40 0.13 ug/L 47753 Perylene-d12 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 8-Benzenesulphonyloxyquinoline 2 di-2-Ethylhexyl chloroformate $$... 185 C12H11NO 192 C9H17C1O2 000000-00-0 47 024468-13-1 43 NO 3 Decanedioic acid, bis(2-ethylhex. .. 426 C26H50O4 000122-62-3 42 4 2-Nonanol, 5-ethyl- (CAS) $$ 5-E... Abundance Scan 2630 (33.400 min): 31585.D (-) 172 C11H240 000103-08-2 38 m/z 185.10 100.00% AAU+ 185

57 5000 112

84 33.00 33.20 33.40 33.60 33.80 oH ........ 207........................... m/z57.10 54.81% mfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #94147: 8-Benzenesulphonyloxyquinoline 57 185

5000 94112 167 33.00 33.20 33.40 33.60 33.80 m/z 71.10 49.65% 0-pmppTT——an!—mmuum00m0mp1 mz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #102311: dl-2-Ethylhexyl chloroformate $$ 2-Ethylhexyl chi... 57 11 2 33.00 33.20 33.40 33.60 33.80 5000 83 m/z 112.10 49.36%

tnfz~> Omnpmp + । 148 192 T—EummmummERTtanmummuaT 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #345444: Decanedioic acid, bis(2-ethylhexyl) ester (CAS) $... I 1 1 > 1 I 1 ' 1 1 1 ' 1 I ' ' ' ' 1 1 ' 185 33.00 33.20 33.40 33.60 33.80 57 m/z 70.10 44.65% 112 5000

0 laylaslyassagdaagod 426 miz—> 40 60 80 100120140160180200220240260280300320340360380400420 33.00 33.20 33.40 33.60 33.80

31585.D SCAN508.M Tue Jan 22 08:36:52 2002 Page 9

NYC-WTC_000049914

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NYC-WTC_000049914Source: NYC Law Department, mirrored locally

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