GCMS analysis results for sample AE00556, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.

NYC-WTC_000051549–000051566

Folder label: “GCMS X 1/9/02 A 1/29/02”

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NYC 9/11 Public Portal Document uilary searen compound Report

Data File : C:\MSDCHEM\1\5973N\O2JAN2 9\00556 . D Vial: 3 • Acq On : 29 Jan 2002 12:12 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-Pentanol, 2,4-dimethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 5.89 3.85 ug/L 1637770 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 36 2 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 33 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 3 - (CYCLOHEX-3'EN-YL) PROPANOL $$... 174 C8H1404 015745-87-6 33 Abundance Scan 220 (5.885 min): 00556.D (-) m/ z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20

m/z-> 4455, T‘‘‘IT ,। , 87 103 । b i'i'i'i ..,. । 11 > ■ ■,

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 । > 11 ■. ■ ।। ■.,, > ।। > j, ।। >,.. । ■ 11 m/z 43.10 25.11% Abundance #17063: 3-Pentanol, 2,4-dimethyl- 73

5000 55 5.60 5.80 6.00 6.20 43 m/ z 45.10 9.61% 27 15 Ji T‘ l‘‘T1‘‘‘‘W‘‘‘‘A‘‘‘O‘1T‘‘1111‘‘‘B1‘I0BU‘IITTTTTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 7)3

5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.02% 55 87 27 45

ti/z-> r " ' i' " ■ i 1 TT i " ■11 ■ ■" 1 i " 111 ■ ■ ■ ■ i' ■ ■ ■ i " " r " ' i ■ " ■ i ■ " ■ i ■ " ■ i ■1" i' " ■ r 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester Bn———————**" 73 5.60 5.80 6.00 6.20 m/z 71.10 6.23%

5000 43 27 55 ■ 1 87 113 174 l'1 11 m-q- T1 ■■I" ''■! T i111 ■ । i ■1" r ■ " i' " ■ r ' " i ■ " ■ r n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

0556.D SCAN508.M Wed Jan 30 09:01:57 2002 Page 7

NYC-WTC_000051559

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NYC-WTC_000051559Source: NYC Law Department, mirrored locally

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