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GCMS blank results for sample AE03510, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.

NYC-WTC_000037680–000037699

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03510.D Vial: 6 Acq On : 8 Mar 2002 2:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 3-Pentanol, 2,4-dimethyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 3.97 ug/L 2124730 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qua 1 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 36 2 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 36 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 Abundance Scan 223 (5.891 min): 03510.D (-) m/z 73.10 100.00% 73

5000 43 __________ . , . । . . . . y, , __ ( , p________ ,.। । , ,,( 5.60 5.80 6.00 6.20 ............. 155.... 11 0 ’ 1’1177117111117 j ni 11 1 87 103 . । tff TTLu]]TUTPU]UUTIWTPNTT) m/z 43.10 25.36% TJz~> 10 20 30 40 50 SO 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17063: 3-Pentanol, 2,4-dimethyl- 73 — — — . i', । 5000 55 5.60 5.80 6.00 6.20 43 m/z 45.10 9.99% 27

L 51 0- 1' I'''' I' " ' 1 * A 1 1 4 11 ।b...।....।....।....।।..n p . i . ।....।.... ।. miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17065: 3-Pentanol, 2,4-dimethyl- 73 r-r. । ■ . . . p-. 5.60 5.80 6.00 6.20 5000' 55 m/z 41.10 9.56% 43 27

miz—> 0- I — 83 TIUUg TTTIOnmE—pmmn 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 34[1,3]dioxolan-2-ylpropyl ester 1 ■ ■ ' ‘ r • ' ‘ T1177 I | I I i r 73 5.60 5.80 6.00 6.20 m/z 71.00 6.63% 5000 43 27 87 , Hp 113 174 0- TPPTTTTT II—55mup—nanur TTuuu ——EEug • * i • • ntz.~> 1C 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

03510.D HP022102.M Fri Mar 15 10:09:05 2002 Page 8

NYC-WTC_000037691

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NYC-WTC_000037691Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

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