GCMS analysis results for sample AE00839, Feb 4 2002

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Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.

NYC-WTC_000052088–000052107

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00839.D Vial: 3 Acq On : 31 Jan 2002 4:21 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 3-Pentanol, 2,4-dimethyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.92 0.40 ug/L 221711 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 36 2 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 36 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 28 4 3-(CYCLOHEX-3’-EN-YL) PROPANOL $$••• 174 C8H14O4 015745-87-6 28 Abundance Scan 223 (5.920 min): 00839.D (-) m/ z 73.10 100.00% 73

5000 43 L ' 5.60 5.80 6.00 6.20 ' ' o1 I 1 ----- 55 ’’11 ... 87... 103 ’I’0111"TTTTTT"-T .............................. ’1’$17’11"T"U-"STSTTTTT*TT’TTTPTTTTT m/z 43.10 24.80% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17065: 3-Pentanol, 2,4-dimethyl- 70

5000 55 dd01n//n—mTnTT 560 5.80 6.00 6.20 43 m/z 45.10 9.18% 27

m/z-> 0 —TTTTT 10 20 30 40 4 44—83.m.. ... 50 i ■ " ' i' ■' ■ i' " ' i 60 70 80 90 100 110 120 130 140 150 160 170 180 pr-n-q-r

Abundance #17063: 3-Pentanol, 2,4-dimethyl- 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.03% 55 43 27

n/z—> 15... Il.... 01'′fr" ' I'’'' I' "'i1 1m 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3Jdioxolan-2-ylpropyl ester —PA4TPAAT 73 5.60 5.80 6.00 6.20 m/z 71.10 6.71% 5000

m/z--> O-p 27 55 . , 87 113 174 THrrpe...... 'I1'1 1 ’' i" 1 r ।" " ।" " i ■ ।" " i"'11" " ।1" 11" " i1" 111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 -A- 5.60 5.80 • • । ■ ■ • • i > < ■ > । 6.00 6.20

00839.D SCAN508.M Fri Feb 01 09:19:13 2002 Page 5

NYC-WTC_000052096

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