Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
NYC-WTC_000037660–000037679Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report • Data File : C:\MSDCHEM\1\5973N\02MAR08\03509.D Vial: 5 Acq On : 8 Mar 2002 1:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-Pentanol, 2,4-dimethyl- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
5.89 3.71 ug/L 1891240 1,4-Dichlorobenzene-d4 9.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 36 2 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 36 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 3-(CYCLOHEX-3 ‘-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 Abundance Scan 223 (5.891 min): 03509.D (-) m/z 73.10 100.00%
L 73
5000 43 15.60 5.80 6.00 6.20 miz-> O . —. 41,55,. 4 1 87 'I. . i . . I1' । 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 .i! 103 । . . . . । . . . . । . . . . । . ■ . . । i .. I । . , . . । ■ . . . । . m/z 43.10 25.48%
L Abundance #17063: 3-Pentanol, 2,4-dimethyl- 73
5000 • • l < ■ • • । • ■ । • ■ 55 5.60 5.80 6.00 6.20 43 m/z •45.10 9.84% 27 1 1 15 0- 11 ' ’ 11'1' i " " i " ■ ‘ i ■ ■' ■ i ■ ■'' i • " ■ i " " I'' " i " " i ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17065: 3-Pentanol, 2,4-dimethyl- 70 ‘ 5.60 5.80 6.00 6.20 5000- 55 m/z 41.10 9.66%
43 27 0- " | “U“ ‘ ‘ 11'" I1 83...................................... . I » t | l. . . j i l t > | < r I I | I i : I J l I l l| > > « ( | i l I • | I I I t | I i l » [ l > i ( | i
mz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester TTpan 73 5.60 5.80 6.00 6.20 m/z 71.00 6.92%
5000
miz-> 0J 27 43
npnpmm ‘I‘552‘‘1‘11101 H87 174 I ' ' TT T 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 113 T^T i ■ “ ■ i ■1 ■' i T — A L 5.60 5.80 6.00 6.20
03509.D HP022102.M Fri Mar 15 10:08:58 2002 Page 10
NYC-WTC_000037673
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NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared topics · similarity 0.997
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Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
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