GCMS blank results for sample AE03615, March 28, 2002

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Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.

NYC-WTC_000037760–000037779

Folder label: “GCMS X 2/19/02 A 3/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03615.D Vial: 5 Acq On : 8 Mar 2002 6:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 3.58 ug/L 1699810 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 0 1 5 7 4 5 - 87 - 6 330 2 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 33 Abundance Scan 223 (5.891 min): 03515.D (-) 73

5000 43 ' ‘ ‘ I ‘ ‘ ' i ‘ ‘ • I ‘ 1 . I I < I t . 5.60 5.80 6.00 6.20 miz-> 0- p-TTT-j-TTTTf m 1 1 55 . 87 103 TT . | > r I I 11 r I TTT | i I > I I. i i . |. I I. i i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 , I. TT r,«■ i. ]. m/z 43.10 25.86% Abundance #36138: 3-(CYCLOHEX-3-EN-YL)PROPANOL $$2-Cyclohexene-1-p... 73

5000 ■ TI TTr 5.60 5.80 4 . 43 m/ z •45.10 9.90%

L 27 55 , 87 113 174 0 TTpmr TI’B’urpr1 101———— 1 I I k 1^'p-T-rrp-TTT-prTT^ , miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17063: 3-Pentanol, 2,4-dimethyl- 73 • • ■ i • TTI * ‘ • TELILTT 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.80% 55 43 27 15 1 1 - —44 — > l 4 I ■ ( 0-'11‘ “' I “ “ I'1 ’.—011111311 rm-pn ’ I —’’11—3/11’1111 ..... 1’111’ mfz~> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxoian-2-ylpropyl ester 73 । TI . Tr TTTmur T f ‘ Tr 5.60 5.80 6.00 6.20 m/z 71.00 6.15%

m/z—> 5000

27 0 TTITITTI 43 8755 113, , 174 TTI i.. ।.. i. ।..., ।.. ।. । ri.. ।.... । ■... ।.... ।.... ।.... ।. ।. ■ ।. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 A5.80 6.00 6.20

03515.D HP022102.M Fri Mar 15 10:09:30 2002 Page 10

NYC-WTC_000037773

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GCMS analysis results for sample AE03617, March 28, 2002 · Box DEP Box 23

NYC-WTC_000037800

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999