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GCMS analysis results for sample AE00839, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.

NYC-WTC_000052088–000052107

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052097
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00839.D Vial: 3 Acq On : 31 Jan 2002 4:21 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.00 1.64 ug/L 904192 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 83 2 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H1202 000123-42-2 83 3 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H1202 000123-42-2 83 4 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 78 Abundance Scan 230 (6,000 min): 00839.D (-) m/z 43.10 100.00% 43

5000 59

101 TITu 5.60 5.80 6.00 6.20 6.40 0........... ,■ i ‘ 1 37,1 51 , ■ । । । ■ ■' i' 1 - 83 125 m/ z 59.10 47.35% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #16600: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 T-Vfl 1 . 59 5.60 5.80 6.00 6.20 6.40 m/z 58.10 17.94% 15 31 101 | 83 | | 0- TTT > - I ' ''I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #16606: 2-Pentanone, 4-hydroxy-4-methyl- (CAS) $$ Diaceton... 43 ’su ’ ’’I" 560 5.80 6.00 6.20 6.40 5000 m/z 101.10 16.70% 59

101

m/z-> 0 1 1 I 1 1 1 1 I ' । 1 । 1T1 10 20 30 40 -H 50 I 60 70 80 83 I ' I ' ' ' ' i ' ' ' ' i ■ ■ ■ 1 p ' ' ' I ' 1 ‘ 1 I 1 1 ' ' i ' ' 90 100 110 120 130 Abundance #16593: 2-Pentanone, 4-hydroxy-4-methyl- (CAS) $$ Diaceton... 1 i ' 1 1 1 i ■ ' ' 1 i ■ ' ' ■ i ' ■ ■ ■ । ■ 43 5.60 5.80 6.00 6.20 6.40 m/ Z 41.10 6.25% 5000 59

31 83 101 /z-> 0 p 10 20 30 40 14 1a1ovitt4v******Ip111411141*//I 50 60 70 80 90 100 110 120 130 AA. TAP . . 5.60 5.80 6.00 6.20 6.40

30839.D SCAN508.M Fri Feb 01 09:19:14 2002 Page 6

NYC-WTC_000052097

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NYC-WTC_000052097Source: NYC Law Department, mirrored locally

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