GCMS analysis results for sample AE00843, Feb 4 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00843 .D Vial: 5 Acq On : 31 Jan 2002 6:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 12 8-Benzenesulphonyloxyquinoline Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 33.40 0.13 ug/L 94750 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 8-Benzenesulphonyloxyquinoline 185 C12H11NO 000000-00-0 50 2 2-cyanomethylene-3-oxo-l,2,3, 4-t... 185 C10H7N3O 000000-00-0 38 3 dl-2-Ethylhexyl chloroformate $$... 192 C9H17C1O2 024468-13-1 35 4 DIISOOCTYL SULFATE 322 C16H34O4S 000000-00-0 32 Abundance Scan 2630 (33.400 min): 00843. D (-) m/z 185.10 100.00% 185

57 5000 70 43 83 112 98 143 33.00 33.20 33.40 33.60 33.80 0- — ■ ■ 11 ■ ■ ■ ■ i • ■ i i ■'' i • ■' ■ r ■' ■ i • ■' i ■ ■ ■ ■ i ■' i 4 m/ z 57.10 52.43%

L n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #94147:8-Benzenesulphonyloxyquinoline 57 185 71

5000 83 94 112 167 T A AALALMAAA 129 33.00 33.20 33.40 33.60 33.80 156 m/z70.10 41.27%

n/z-> 0- ' i ■ ■' ■ i ■' ■ ■ i ’ • ■ ■ i ■ ■ ■ ■ i' 40 50 i ■ ■ ■ ■ i 60 70 80 90 100 110 120 130 140 150 160 170 180 190 i• • ■ ■ i • • i A Abundance #93917: 2-cyanomethylene-3-oxo-1,2,3,4-tetrahydroquinoxaline 185 WM 33.00 33.20 33.40 33.60 33.80 5000 m/Z71.10 39.21% 157

81 90 103 . n/z-> 0 ' l1' •11' ’'' I " ’' I' 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 I Abundance #102311: dl-2-Ethylhexyl chloroformate $$ 2-Ethylhexyl chi... ITT ■ i ■ ■ 57 70 112 33.00 33.20 33.40 33.60 33.80 m/ Z 55.10 27.30% 5000 83

i 97 0 '' I'''11'' TIP Irry 1" 111 ■' ।11 ■11"148 " i' i ’ ■ " i1 ■ ■ ■ i 192 ■ i' ■ " i /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 33.00 33.20 33.40 33.60 33.80

00843.D SCAN508.M Fri Feb 01 09:19:29 2002 Page 14

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