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GCMS surrogate recovery results for sample AE00279, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00279 analyzed on January 10, 2002.

NYC-WTC_000050875–000050892

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050884
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library searen compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN09\279.D vial: 4 Acq On 9 Jan 2002 8:40 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2-Buten-l-ol, 2-methyl- (CA... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

4.63 0.15 ug/L 69546 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Buten-l-ol, 2-methyl- (CAS) $$... 86 C5H10O 004675-87-0 43 2 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 38 3 Ether, hexyl pentyl $$ Hexane, 1... 172 C11H240 032357-83-8 38 4 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 35 Abundance Scan 110 (4.630 min): 279.D (-) m/ z 71.10 100.00% 41 57 71

88

5000

101 TBT 1A— n/z-> 0- ■ । 10 ' 1 । ■ ■ ■ ■ । ■ 20 30 40 J—7ll I... I 50 60 70 ' I ' ' ' ' I ' 80 90 100 110 — 120 4.20 m/z 4.40 41.10 4.60 4.80 94.55% 5.00

Abundance #4064:2-Buten-1-ol. 2-methyl- (CAS) $$ 2-Methyl-but-2-ene... 71

5000 43

53 86 ANMA 4.20 m/z 4.40 57.10 4.60 4.80 92.62% 5.00 £

................... . 0—T ■ i • > • > i ■ • ■ ■ । > 4T /z-> 10 20 30 40 50 60 701 80 90 100 110 120 Abundance #16440: Butanoic acid, 2-methyl-, methyl ester (CAS) $$ Me... 57 88

4.20 4.40 4.60 4.80 5.00 5000 m/z 88.10 67.85% 101 74 27 15 I 01 ' I ' ' ' ' I ' 1............. ' ' I ' ' ' ' I ' ' ' ' I 1 ■ i ■ ■ ' ■ i ' n-1 j___________ । ■ ■ ■ ■ । —r 1 116 I 1 1 ' ' I 1 1 m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 #76907: Ether, hexyl pentyl $$ Hexane, l-(pentyloxy)- 110 120 . ....... W 43 4.20 4.40 4.60 4.80 5.00 m/z 43.10 58.76% 71 5000

n/z-> 0 10 20 30 40 ‘ I’’ 50 56

IL ' ' 'll'.. ■'! ' ' 60 70 80 85

90 101 100 110 120 4.20 WM 4.40 4.60 4.80 A 5.00

279.D SCAN508.M Thu Jan 10 11:51:49 2002 Page 5

NYC-WTC_000050884

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NYC-WTC_000050884Source: NYC Law Department, mirrored locally

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