GCMS surrogate recovery results for sample AE00279, Jan 2002

NYC 9/11 Public Portal Document LLDLaiy ~upouru RpUit

Data File : C:\MSDCHEM\1\5973N\02JAN09\279.D Vial: 4 ‘ Acq On 9 Jan 2002 8:40 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 4-O-Methyl-d-arabinose Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

4.24 0.12 ug/L 56341 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 4-O-Methyl-d-arabinose 164 C6H12O5 000000-00-0 50 2 N,N'-Diacetylethylenediamine $$ ... 144 C6H12N202 000871-78-3 16 3 (2-Methyl-oxetan-2-yl)-methyl-1,... 172 C9H16O3 114872-47-8 16 4 THIOPHENE-DI 85 C4H3DS 000000-00-0 10 Abundance Scan 76 (4.241 min): 279.D (-) m/z 43.00 100.00% 48 87

5000 55

w .6, (A M 3.80 4.00 4.20 4.40 4.60 0 . • । . . • • । । । j m/ z 87.10 95.96% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #63795: 4-0-Methyl-d-arabinose 87

5000 60 1 I 11 1 1 I 1 3.80 4.00 4.20 4.40 4.60 m/z 89.10 63.59% 74

OTT ■ i ■ ■ ■ ■ i ' I. I 100 , 117..128, m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #39767: N,N'-Diacetylethylenediamine $$ Acetamide, N.N-1.... 43 30 85 3.80 4.00 4.20 4.40 4.60 5000 73 m/z 85.00 55.82%

15 60 01 ......................... - , 1 , 11, . . ....... rn/z--> Abundance 10 20 ■ ■ । 30 40 50 60 70 80 #76041: (2-Methyl-oxetan-2-yl)-methyl-1,4-dioxane 87 90 100 110 120 130 380 4.00 AN.. A, 4.20 4.40 4.60 43 m/z 41.10 47.56%

5000 31 71

56 0 ■ •। ■ • ■ •। • ■ •■ । Il I II ■ ■ । ■ ■ ■ ■ । ■ ■ ’ 'I ' ' ' ' I ' ' ' ' I ' ' I ' 1 ' ' I ' ' ■ ■ I ■ ' ■ ' I ■ ' ' b I ' 1 rn/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 3.80 4.00 4.20 4.40 4.60

279.D SCAN508.M Thu Jan 10 11:51:49 2002 Page 4

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