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GCMS surrogate recovery results for sample AE00281, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.

NYC-WTC_000050912–000050931

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050920
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\5973N\O2JANO9\281.D Vial: 6 Acq On : 9 Jan 2002 10:21 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 4-O-Methyl-d-arabinose Concentration Rank. 11

R.T. EstConc Area Relative to ISTD R.T.

4.24 0.11 ug/L 62684 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-O-Methyl-d-arabinose 164 C6H1205 000000-00-0 9 2 l-Cyano-2-mercapto-ethane 87 C3H5NS 000000-00-0 4 3 Ethane, isothiocyanato- (CAS) $$... 87 C3H5NS 000542-85-8 4 4 1-Pentanamine (CAS) $$ n-Amylami ... 87 C5H13N 000110-58-7 4 Abundance Scan 76 (4.241 min): 281 .D (-) m/z 87.10 100.00% 87

43 55 5000 / rr 1 ""I 3.80 4.00 4.20 -rA . . 4.40 4.60

n/z-> 0+ ri'1'■i' ■ ' 1 i' 20 30 40 49 50 1... ....-Il 60 70 80 90 100 110 120 130 m/ z 89.10 73.26% Abundance #63795: 4-0-Methyl-d-arabinose 87

5000 60 3.80 4.00 4.20 4.40 4.60 m/z 55.10 60.33%

m/z-> Abundance o 20 30 40 l 50 60 - 70 74

80 100 117 *Tn—u—u———3tiueu—ir 90 #4324: 1-Cyano-2-mercapto-ethane 100 110 120 128 130

87 47 - --- PA, 3 80 4.00 4.20 4.40 4.60 5000 m/z 43.10 57.86%

/z-> 0 T-J-I

Abundance 20 26 53 59

1 i ' r ■ ' i ' ' ' ' i ■ 30 40 50 60 70 80 90 100 #4319: Ethane, isothiocyanato- (CAS) $$ Ethyl isothiocyana... 110 120 130 ft ISlAl 59 87 3 80 4.00 4.20 4.40 4.60 29 m/z 41.10 29.32% 5000 72

/z—> 0 ■ i ■ ■ ' 1 । 1 ■ ■ ' i ■ 20 30 40 44

50 r 60 .-I170!-. 80 --------- 90 100 110 120 130 N Nwy 380 4.00 4.20 4.40 4.60

il.D SCAN508.M Thu Jan 10 11:52:00 2002 Page 4

NYC-WTC_000050920

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NYC-WTC_000050920Source: NYC Law Department, mirrored locally

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