GCMS surrogate recovery results for sample AE00281, Jan 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN09\281.D Vial: 6 Acq On : 9 Jan 2002 10:21 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 3.49 0.15 ug/L 81193 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 83 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 4 Dichloroacetonitrile $$ Acetonit...109 C2HC12N 003018-12-0 38 Abundance Scan 10 (3.488 min): 281 .D (-) m/z 74.00 100.00% 74

82 5000

47 ' 1 1 1 1 ■ i 1 ' ' ■ i k * * ’ i * ’ *4 । ■ ’ 39 3 50 3.60 3.70 3.80 3.90 0 1 i ' ■ 1 ■ i 1 spP-ll, 4Hbu,pr I i ' | l ■ ■ ■ | • 1 1 | ‘ “r m/z 81.95 50.89% /z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11644: Acetonitrile, dichloro- 74 35

5000 82 I ' ■ ' ■ I "r ' ' 'I 11 3.50 3.60 3.70 3.80 3.90 47 m/z84.00 32.44% 01 T-rT-r-r TTT Trilmr ri ■ i > > ‘ > i » । • i < ■ ■ ■ । ‘ । । m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 76.00 29.36% 47 35

m/z-> 0t ............. I,..... .. 60 10 20 30 40 50 ■' i ' 1 1 ■ i ■ 70 80 1 90 100 9— +1110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... "T -----PPPA 74 3.50 3.60 3.70 3.80 3.90 82 m/z 47.00 24.62% 5000 47

n/z-> 0 12 1 r ' I 1 1 1 ' i 1 ' ■ ■ i 1

10 20 30 35 - 40 -hmmPp 50 60 70 TTt 80 । ' 1 1 1 1 1 1 1 1 ' ' 1 I ' ■ 90 100 108 110 N.,........... y 3.50 3.60 3.70 3.80 3.90

1 .D SCAN508.M Thu Jan 10 11:51:59 2002 Page 3

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