GCMS analysis results for sample AE00844, Feb 26 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00844.D Vial: 7 Acq On : 7 Feb 2002 7:24 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP020702.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

3.50 0.13 ug/L 50567' 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 74 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 56 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 43 4 Dichloroacetonitrile $$Acetonit... 109 C2HC12N 003018-12-0 37 Abundance Scan 11 (3.499 min): 00844.D (-) m/z 74.00 100.00% 74 82 5000 47 38 3.50 3.60 3.70 3.80 3.90 0 ................ 1,1, ' I III, ' ' +I‘‘‘‘IU 1 ' i ■ ■ ■ ‘ i ■ ■ ■ ' i ' m/z 81.90 56.23% n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 7l4

5000 82 ‘ IT* । "TTTTTTTromr 3.50 3.60 3.70 3.80 3.90 47 m/ z 84.00 39.76% 35

m/z-> Abundance 01 ...... 10 Hp 20 30 40 50 60

35 TTI • i > > > • i ■ 70 80 #11644: Acetonitrile, dichloro- i

714

82 । '90- -100-—199, 110

J 1tII**IIv*****v‘I****/‘*‘‘I 3.50 3.60 3.70 3.80 3.90 m/ z 76.00 34.52% 5000

47

m/z-> O+ ' ' i ' ' ' ' i ■ ' ' ■ i ■ ' । 10 20 30 — 40 m 50 60 TO3I 1—1—————————— ■ ' । '1 '1 । ■ 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 1‘111111‘10010*t1‘‘‘0*‘1 74 3.50 3.60 3.70 3.80 3.90 82 m/ Z 47.00 22.63%

5000 47 35 0 ...2......... ....... III,... 11‘ ‘IS ‘ 1 । 108 mfe-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90

00844.D HP020702.M Thu Feb 21 09:58:16 2002 Page 3

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