GCMS analysis results for sample AE00559, Jan 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00559.D Vial: 3 Acq Cn : 15 Jan 2002 3:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.48 0.18 ug/L 54450 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 74 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 74 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 64 Abundance Scan 9 (3.476 min): 00559.D (-) m/z 74.00 100.00% 74

82 5000 47 38 3.50 3.60 3.70 3.80 3.90 O- -4 I'"'I'"'I - T**uuuuun m/z 82.00 52.19%

A7100 .... m/z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

5000 82 3.50 3.60 3.70 3.80 3.90 47 35 ■ ■ u।| ■11 >| " 111 109 0 r■"r'"I T TTT’ P—r m/z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #11644: Acetonitrile, dichloro- 7)4 35 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 76.00 27.72% 47 40 0 T 11111111...111।1111 111" TTIT Tt i ■" ' r "11 I " " r " 1111 m/z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... '11’7 1111 > > > r > ‘ ' 11 ■ ।' । 74 350 3.60 3.70 3.80 3.90 m/z 47.00 25.26% 47 82 5000

38

m/z—> 0 " r 1" 11 ■ i1 "' i' mm , TTV 1 । | । 'l' | 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 95 1"102 108 I I I |TI I I | I I I I | I I TIT 3.50 3.60 3.70 3.80 3.90 a 00559.D SCAN508.M Wed Jan 16 08:14:05 2002 Page 3

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