GCMS analysis results for sample AE03185, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03185 conducted on March 15, 2002.

NYC-WTC_000006065–000006084

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document — 2

Data File: C:\MSDCHEM\1\5973N\02MAR01\03185.D Vial: 5 • Acq On : 1 Mar 2002 1:38 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 3.50 0.13 ug/L 50854 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 78 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 50 4 Dichloroacetonitrile $ $ Acetonit... 109 C2HC12N 003018-12-0 42 Abundance Scan 11 (3.498 min): 03185. D (-) m/z 73.95 100.00% 74 82 5000

47 1 ' i ■ ' ■ ■ i r ' 3.50 3.60 3.70 3.80 3.90 Of ■ > i ■ > < > I । । 1"1 lHe 1 I 1 1 ‘ ' I 1 I i ■ i ■ ■ ■ । i 1 1 1 ' i 1 । m/z 81.90 57.68% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11644: Acetonitrile, dichloro- 7|4 35

5000- 82 M..... 3.50 3.60 3.70 3.80 3.90 47 m/z 83.90 30.98% 01 1 1 I 1 1 1 ' I 1 1 ' 1 1 1 11 t 1 411) ' 1 _________________ L 1 1 I ' ' ' 1 1 1 TII 1 ■ i 1 1 ■ 1 i ■ ■ 1 ' i ' 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

3.50 3.60 3.70 3.80 3.90 5000 82 m/ z 76.00 28.72% 47 35 1 1 1 1 ' ' ' I 1 1 ' - ' , ] > i >' 111 i । , i । > । > > । >1 n/z-> Of 10 20 30 40 50 60 70 TIit 80 90 1 —.. 109 100 110 ' Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... ■ ■ i ■ i ■ 1 ■ ' i ' ' ' 1 i 74 3.50 3.60 3.70 3.80 3.90 82 m/ z 47.00 20.85%

5000 47

n/z-> 12 0 1 1 1 । I 1 1 10 ....... 20 30 ,110 40 35 —50PIPTmIn 60 70 80 108 1 i 1 1 ■1 i 1 1 1 1 I ' 1 90 100 110 a TIIttTTTI1r-1111111 3.50 3.60 3.70 3.80 3.90 n Ju )3185.D HP022102.M Mon Mar 04 12:32:59 2002 Page 3

NYC-WTC_000006071

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