GCMS analysis results for sample AE01140, Feb 2002

NYC 9/11 Public Portal Document

: C:\MSDCHEM\1\5973N\02FEB25\01140.D Data File Vial: 6 Acq ’ On: 25 Feb 2002 3:22 pm Operator: • ' Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 3.50 0.27 ug/L 104727 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 74 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 72 4 Dichloroacet onitrile $$ Acetonit... 109 C2HC12N 003018-12-0 38 Abundance Scan 11 (3.498 min): 01140.D (-) m/z 74.00 100.00% 74 82 5000

47 .... R........ 3.50 3.60 3.70 3.80 3.90 01 10 * 20 30 40 150. 60 70 80 1 ■ i ■ ■ ■ 1 i ■ ■ ■ 1 । 1 1

90 100 110 m/z 81.90 58.75% m/z-> Abundance #11644: Acetonitrile, dichloro- 74 35

5000 82 AN... I ' ' 1 1 I 3.50 3.60 3.70 3.80 3.90 47 m/ z 83.90 32.14%

m/z-> Of ■ ' i ■ ■ ■ ' i ' ' 1 ■ i 1 ■ 1 1 I ' 10 20 30 40 +50— 60 1 1 I ' ' ' ' 1 1 70 I

80 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

3.50 3.60 3.70 3.80 3.90 5000 82 m/z 76.00 29.17% 47 35

m/z-> 0! ........................... | 10 20 30 40 n50............ 60 70 1 1[B 80 HP 90 199— 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82 3.50 3.60 3.70 3.80 3.90 m/z 47.00 21.41% N 5000 47

miz-> 0 1 . ................. 10 20 ..35...... Ill,.. 30 40 50 ■ । ■ ■ ■ 1 । ■ 60 70 । 1—r* 80 II ■ । ■ ■ ■ ■ । 90 100 108 । । > I ■ ' 110 MN 3.50 3.60 3.70 3.80 3.90

01140.D HP022102.M Tue Feb 26 08:30:17 2002 Page 3

NYC-WTC_000003509