GCMS analysis results for sample AE00320, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN08\320.D Vial: 5 Acq On : 8 Jan 2002 8:47 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 4-0-Methyl-d-arabinose Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

4.23 0.11 ug/L 38076 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 4-0-Methyl-d-arabinose 164 C6H1205 000000-00-0 64 | 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 V 3 Glycine, methyl ester $$ NH2CH2C... 89 C3H7NO2 000616-34-2 5 4 1-Pentanamine (CAS) $$ n-Amylami... 87 C5H13N 000110-58-7 4 Abundance Scan 75 (4.230 min): 320.D (-) m/z 87.10 100.00% 87 55 43 5000 .................... ...........................

3.80 4.00 4.20 4.40 4.60 0 ■ I ■ ■ « > । । ■ i • ■ i ■ ■ ' ■ i ■ ■ ■ ■ । ■ 1 1 ■ । ' 1 1 ■ i ■ ■ ■ ■ । ■ ■ ■ • i ' ' ' ' । ■ ■ ' • । ' m/z 89.00 78.91% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #63795:4-0-Methyl-d-arabinose 87

5000 60 3.80 4 00 4.20 4.40 4.60 45 m/z 55.10 66.10% 74

o1 .......... 1.1...... 100 ..... II...... 111tsl--**u 117 128 ‘‘*‘i..... /z-> 20 30 40 50 60 70 90 100 110 120 130 80 Abundance #4415:1-Butanamine, 3-methyl- 33

3.80 4.00 A... -4 4.20 4.40 4.60 5000 m/ z 43.00 51.91%

41 55 70 87

| aA 0—T -------- n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5025: Glycine, methyl ester $$ NH2CH2COOCH3 89 3.80 4.00 4.20 4.40 4.60 m/z 59.10 18.20%

5000 44 . 59

n/z-> 0—11 20 30 66 n-' 40 50 60 70 80 90 100 110 120 130 3.80 4.00 4.20 4.40 4.60

320.D SCAN508.M Wed Jan 09 15:18:11 2002 Page 3

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