GCMS analysis results for sample AE03075, March 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB28\02714.D Vial: 4 Acq On : 28 Feb 2002 1:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Glycine, methyl ester $$ NH... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.25 0.16 ug/L 60747 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Glycine, methyl ester $$ NH2CH2C... 89 C3H7NO2 000616-34-2 9 2 3,5,5-Trimethyl-l-n-butyl-3,4-di... 172 C8H20N4 000000-00-0 9 3 Diazene, butyl[1-(2,2-dimethylhy... 172 C8H20N4 061940-95-2 9 4 1-Pentanamine (CAS) $$ n-Amylami... 87 C5H13N 000110-58-7 9 Abundance Scan 78 (4,254 min): 02714.D (-) m/z 87.00 100.00% 43 87

55 50001 i \ 59 4.00 4.20 4.40 4.60 47 Of • • i • ‘ ‘ i • • ” i' *' • i i11" i" i “ ’ • l • • * • i • ‘ ' i ‘ •11 ■ * p-m-p-r m/z 89.00 96.89% miz-> 20 253035404550556065 70 75 80859095 Abundance #5025: Glycine, methyl ester $$ NH2CH2COOCH3 89

5000 ■ ' i ■ • ■ ■ i ■ ■ ■ 1 i ■ ■ ‘ ■ i ■ 1

44 4.00 4.20 4.40 4.60 m/ Z; 43.10 96.57% 59 A m/z-> 0) • ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ —P+ 90 20 25 30 35 40 45 50 55 60 65 70 75 80 85 -i-p-r 95 Abundance #75878:3,5,5-T rimethyl-1 -n-butyl-3,4-dihydroformazine 44 87 AAA 4.00 4.20 4.40 4.60 5000 m/z 55.10 64.85%

59 A 30 Of -H ' i1 ■ ■ ■ i ■ H 71 I Hp miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #75870: Diazene, butyl[1-(2,2-dimethylhydrazino)ethyl]- 44 87 0.0 ........ 4.00 4.20 4.40 4.60 m/z 41.10 54.72%

500)

iz—> o-p]. 30 +5 11111111 +mmp 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 59 — AA 4.00 4.20 4.40 4.60

02714.D HP022102.M Fri Mar 01 10:07:00 2002 Page 6

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