GCMS analysis results, Feb 27 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01138.D Vial: 4 : Acq On : 25 Feb 2002 1:43 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-METHYL-3,3-D2-AZIRIDINE Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

9.89 0.11 ug/L 42544 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 4 2 Butane, 2-methoxy- $$ Ether, sec... 88 C5H120 006795-87-5 4 3 Acetamide (CAS) $$ Ethanamide $$... 59 C2H5NO 000060-35-5 4 4 Butane, 2-methoxy- (CAS) $$ Meth... 88 C5H120 006795-87-5 4 Abundance Scan 577 (9.887 min): 01138. D (-) m/ z 59.10 100.00% 50

5000

Or 41 45 -49 hr 73 - 86 M 9.60 m/ z 9.80 45.10 10.00 10.20 14.78% mlz~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #500: 2-METHYL-3,3-D2-AZIRIDINE 20 58

5000 ... JI 9.60 9.80 10.00 10.20 42 m/ z -41.10 13.03% 26 oh 2 - TTTp- ^illl,....... 1111111111200111 n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4938: Butane, 2-methoxy- $$ Ether, sec-butyl methyl $$ se... 50 9.60 9.80 10.00 10.20 5000 m/ z 73.00 12.74%

15 27 31 45 73

n/z-> Of" " i ■" TIT „54 I 88 I" " r ‘'11" 111" “ i" " r " ' r1" i" 5; 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #641: Acetamide (CAS) $$ Ethanamide $$ Acetic acid amide $... 50 —9.60 A 9.80 M. 10.00 10.20 44 m/ z 85.90 10.61%

5000

41 Oh TI00111—0001—0011—B-0—mm7or I'1" i" " i" " i ■" ■ i ■ " ' i1 ■ ■' i " " i" miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 9.60 9.80 10.00 10.20

01138.D HP022102.M Tue Feb 26 08:30:03 2002 Page 11

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