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GCMS analysis results, Feb 27 2002

Machine-extracted title · confidence 90%

Gas chromatography-mass spectrometry results for sample AE01138 identifying unknown compounds and surrogates on February 27, 2002.

NYC-WTC_000003463–000003482

Folder label: “GCMS X 1/20/02 A 2/25/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01138.D Vial: 4 ■ Acq On : 25 Feb 2002 1:43 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Cyclopentasiloxane, decamet... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

12.54 0.09 ug/L 47747 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 3 1,1,3,3,5,5,7,7,9,9,11,11,13,13-... 504 C14H4406Si7 000000-00-0 38 4 Heptasiloxane, 1,1,3,3,5,5,7,7,9. . . 504 C14H4406Si7 019095-23-9 38 Abundance Scan 812 (12.540 min): 01138. D (-) m/ z 73.00 100.00% 73

5000 267 355 - 45 12.20 12.40 12.60 12.80

m/z-> 0 XU I I ..... । ' I " " I " " I " " I ' " ' I ‘ " I ' ‘ " I ' ‘ 1 ' I " " I' ' " I'’ " I" " I 40 60 80 100120140160180200220240260280300320340360380400420 .. Hir 11 ■" ‘ i" ■11 m/z 355.00 42.68% Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 ' I ' 1 ' 1 1 1 ' ' 1 I 12.20 12.40 12.60 12.80 355 m/ z 266.90 39.62% 45 __ 193 223 249 i 323 0 TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT TTTTTTTT m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #313068: Cyclopentasiloxane, decamethyl- 73 ' 1 i i ■ ■ ■ ■ I 355 12.20 12.40 12.60 12.80 267 m/ Z 356.10 12.74% 5000

207 2491 323 l 0 1I—20093000TBB10"0101310EE1"011110111101111411111171191 ।■ i ■ ■ ■ • । >i■■■■i m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #369234:1,1,3,3,5,5,7,7,9,9,11,11,13,13-TETRADECAMETHYL-H... ' ' I ' 1 1 ' 1 1 ' 11’I’I’I 73 12.20 12.40 12.60 12.80 m/ z 357.00 11.03%

5000 207

133 281 355 0 TT mmmm It........ 1......327.1 TTTTTTTTTTTTT 429 ............... .. ■ ■ 1 i ' ■ ' ■ i ' ' 1 ■ i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 12.20 12.40 12.60 12.80

01138.D HP022102.M Tue Feb 26 08:30:04 2002 Page 12

NYC-WTC_000003478

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NYC-WTC_000003478Source: NYC Law Department, mirrored locally

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