GCMS analysis results, Feb 27 2002

NYC 9/11 Public Portal Document

Data File: C:\MSDCHEM\1\5973N\02FEB25\01138.D Vial : 4 .. Acq On : 25 Feb 2002 1:43 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 2,5-Cyclohexadiene-1,4-dion... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

13.38 0.06 ug/L 32184 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Cyclohexadiene-l,4-dione, 2 , ... 140 C6H404 000615-94-1 64 2 l-Oxetan-2-one, 4,4-diethyl-3-me... 140 C8H1202 000000-00-0 64 3 2 -Methoxy-3 -hydraziny1-pyrazine 140 C5H8N40 000000-00-0 64 4 Flamenol $$ 5-Methoxyresorcinol ... 140 C7H803 002174-64-3 9 Abundance Scan 886 (13.376 min): 01138. D (-) m/z 140.00 100.00% VO

5000 ,................................................. 70 54 94 13.00 13.20 13.40 13.60 13.80 0 a 84| ..... .............. I, 161 m/ Z 70.00 20.12% m/z-> 30 40 50 60 7080 90 100 110 120 130 140 Abundance ;#35123: 2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- VO

42 5000 TIT ■ ' i ' ■ ■ ■ i ■ 69 13.00 13.20 13.40 13.60 13.80 84 m/Z 141.10 12.15% 53 01 i 1 1 • । i .... .... I. TTT ----- 94 112 I 1tT m/z-> 30 40 50 60 7080 90 100 110 120 130 140 Abundance #35765: 1-Oxetan-2-one, 4,4-diethyl-3-methylene- 79 VO 39 67 ' i ' 1 ' ■ i ■ ■ 11Il । । । । । 13.00 13.20 13.40 13.60 13.80 125 m/ Z 93.90 10.16% 5000 53 111 97

| | 0 1 1 i 1 T7T mlz—> 30 40 50 60 70 80 90 100 110 120 130 140 ----- Abundance #35089:2-Methoxy-3-hydrazinyl-pyrazine VO 13.00 13.20 13.40 13.60 13.80 m/z 96.00 10.13%

5000 42 54 68 80 95 108 121 ill II .... I I 0 1 ■ ।' ’ 1* ........ TIT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

01138.D HP022102.M Tue Feb 26 08:30:04 2002 Page 13

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