GCMS analysis results for sample AE03251, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03251 conducted on March 15, 2002.

NYC-WTC_000006206–000006225

Folder label: “GCMS X 2/12/02 A 3/01/02”

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Data File: C:\MSDCHEM\1\5973N\02MAR01\03251.D Vial: 6 - Acq On : 1 Mar 2002 8:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 2-Methoxy-3-hydrazinyl-pyra ... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.06 ug/L 36559 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 64 2 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 50 3 l-Oxetan-2-one, 4,4-diethyl-3-me... 140 C8H1202 000000-00-0 9 4 Flamenol $$ 5-Methoxyresorcinol ... 140 C7H803 002174-64-3 9 Abundance Scan 886 (13.376 min): 03251.D (-) m/z 140.00 100.00% 140

5000 ....................... ,.......................... 70 94 13.00 13.20 13.40 13.60 13.80 0-P— 49..... |, 84,11........................ 1 1 ' 1 1 ' I ' 1 dpm/ I I | I I I ! | I I I I | I I T"T m/Z 141.00 14.35% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35089: 2-Methoxy-3-hydrazinyl-pyrazine 140

5000 42 13.00 13.20 13.40 13.60 13.80 54 68 m/ z 70.00 12.84% 80 95 108 121

m/z-> 9i ' 1 1 1 30 40 ■ 1 i 1 50 60 ‘ ' 1 1 1 70 80 I,....1.... 90 100 110 120 130 ■ r i ■ ■ ■ > । । ■ —1 TTI 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140 ■ i ■ ■ ' i ■ ■ N.... 1 ' I ‘ 1 1 1 1 1 13.00 13.20 13.40 13.60 13.80 5000 m/z 94.00 10.53% 44 71 123

m/z—> 0 TTn 30 — 40 ' i ■ ' ' ' i ' ■ 50 60 1l 70 80 90 86 96 ------- 100 112 110 120 130 l 140 ■’“T

Abundance #35765:1-Oxetan-2-one, 4,4-diethyl-3-methylene- 79 140 13.00 13.20 13.40 13.60 13.80 39 67 m/ z 66.00 9.09% 125 5000 53 111 97

0 l ■ ■ • l l ■ ■ ■ 1 i ■ 1 ■ 1 i 1 1 1 1 i 1 1 ^r1 —— ....... .. TII m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

33251.D HP022102.M Mon Mar 04 12:33:48 2002 Page 12

NYC-WTC_000006221

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