GCMS analysis results for sample AE03251, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03251 conducted on March 15, 2002.

NYC-WTC_000006206–000006225

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document 2 puli LDOL

Data File : C: \MSDCHEM\1\5973N\02MAR01\03251.D Vial: 6 • Acq On : 1 Mar 2002 8:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Cyclopentasiloxane, decamet... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.25 ug/L 152078 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- ... 370 C10H3005Si5 000541-02-6 83 2 6-Aza-5,7,12,14-tetrathiapentacene 355 C17H9NS4 000000-00-0 78 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 4 Phenethylamine, N-methyl-.beta.,.. . 399 C18H37NO3Si3 010538-85-9 47 Abundance Scan 812 (12.540 min): 03251 .D (-) m/ z 73.00 100.00% 73

355 5000 267 - 45 12.20 12.40 12.60 12.80 I. 0 -----PPP 191 207 1541WPTITIIIT 251 || 323339 TITTTTITTTTT TIT m/z 355.00 53.60% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313067: Cyclopentasiloxane, decamethyl- $$ Decamethylcycl... 355

73 267 5000 .mm.... 12,20 12,40 12.60 12.80 m/ z 266.90 47.16% 193 223 251 323339 0 T1WTITIIWTTTDTITWTLWWIWIWIIPNITTTTT -TT I’I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #302266: 6-Aza-5,7,12,14-tetrathiapentacene 355 ‘tt ■ i ' ' ' ' i 12.20 12,40 12.60 12.80 5000 m/z 356.00 15.58% 291 323

0 1111'' । <1 ■ । । ।।। ■ 111 ■ 11' 1111111. < 11 > । । > 11 ITT 111111111111 P lz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313066: Cyclopentasiloxane, decamethyl- ....... 1 1 । ■ 1 ' ■ । ■ 1 1 1B‘ 1 ' 1 1 1 ' ■ I 355 12.20 12.40 12.60 12.80 73 m/z 267.90 12.92% 267 5000

193 251 li 323339 0 ' i' " ' r ' " i " ' i ‘ " 111 " 11 ■' " I " '' i' " ' i'' i ■ — — 1’1 i ■ ■ ■ ' । ■ 1 1 । m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80

33251.D HP022102.M Mon Mar 04 12:33:48 2002 Page 11

NYC-WTC_000006220

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NYC-WTC_000006220Source: NYC Law Department, mirrored locally

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