GCMS analysis results for sample AE03251, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03251 conducted on March 15, 2002.

NYC-WTC_000006206–000006225

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document X wpulit LCDUL

Data File : C: \MSDCHEM\1\5973N\02MAR01\03251.D Vial: 6 Acq On 1 Mar 2002 8:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 3.68 ug/L 1533000 1,4 -Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3 ’-EN-YL)PROPANOL $$. . . 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 17 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 223 (5.891 min): 03251.D (-) m/z 73.10 100.00% 7)3

5000

43 5.60 5.80 6.00 6.20 0- . ...... 1,1,11125811117 TTTTTTTTTTTTTTETTTLTTTTEOTTTTTTTTTITTTTTT , 87 103 m/z 43.10 24.47% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3‘-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 5.60 5.80 6.00 6.20 43 m/ z -41.10 9.09% 27 55 87 113 174 , i 0 " i11111' " ' r TT4 ' i " " i " 1 'i' Pp ■''' ।1'1 r ।" ■11 ' i " " i " " i'1" i " " i" " i "111 ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 . A) . rfir 5.60 5.80 6.00 6.20 5000 m/ Z 45.10 8.86% 43 27 55 . 87 TTTTTTTTT Ii " " I " " 113 01" i " ‘' i ■ " 11 ‘' 174 i1' " i " " i " " i'' " i " " r " 11" " i ‘ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 70 5.60 5.80 6.00 6.20 m/z 71.00 6.72% 5000

45 15 | 53

m/z-> 0 nijunipa .. TTTHTTTT 88 '11" " i " ‘' i " 1' r 1 .......... ..।।।. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80

33251 .D HP022102.M Mon Mar 04 12:33:48 2002 Page 10

NYC-WTC_000006219

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