GCMS analysis results for sample AE01140, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01140.D Vial: 6 Acq ‘ Cn : 25 Feb 2002 3:22 pm Operator: • ' Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 11 2-Methoxy-3-hydrazinyl-pyra... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

13.38 0.05 ug/L 28152 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 83 2 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N2O2 004212-49-1 64 3 l-Oxetan-2-one, 4,4-diethyl-3-me... 140 C8H12O2 000000-00-0 64 4 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 64 Abundance Scan 886 (13.376 min): 01140.D (-) m/z 140.00 100.00% 14.0

5000

66 94 108 13.00 13.20 13.40 13.60 13.80

/z—> 0 1 30 40 50 60 70 80 - 90 100 110 120 130 | 140 ‘ .1 m/z 94.00 11.88% Abundance #35089:2-Methoxy-3-hydrazinyl-pyrazine 140

5000 42 TIB TfITT 13.00 13.20 13.40 13.60 13.80 54 68 m/Z 66.00 11.10% 80 95 108 121

m/z—> o1, .... 11 30 40 1 ' I ' 50 ' 60 ' 70 80 90 .... 1...... 11..... 140I 100 110 120 130 TII

Abundance #35153: Uracil, 5-ethyl-$$ 2,4(1 H,3H)-Pyrimidinedione, 5-... 140 125 82 13.00 13.20 13.40 13.60 13.80 5000 m/z 108.10 11.01%

54 68 96 0 । ■ . ■ > । ■ . ■ ■ । > I ■ . । > I | ■ • ■ ■ f I. 111 TImmpr +tt TIT m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35765: 1-Oxetan-2-one, 4,4-diethyl-3-methylene- TIit 'I I I I 1 1 1 1 1 1 1 1 79 140 13.00 13.20 13.40 13.60 13.80 39 67 m/ Z 70.10 10.80% 125 5000 53 111 97

------------------ 0- TTT m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

01140.D HP022102.M Tue Feb 26 08:30:18 2002 Page 13

NYC-WTC_000003519