GCMS analysis results for sample AE01140, Feb 2002

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Laboratory report documenting GCMS analysis of sample AE01140 conducted on February 27, 2002.

NYC-WTC_000003503–000003522

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01140.D Vial: 6 Acq Cn : 25 Feb 2002 3:22 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 N-perdeuteriobenzylideneani ... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 86825 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 53 2 Pyrazine, tetraethyl- (CAS) $$ t... 192 C12H20N2 038325-19-8 50 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 42 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 Abundance Scan 1675 (22.283 min): 01140.D (-) m/z 192.00 100.00% 192

5000

96 AO AK 82 146 160 . 22.00 22.20 22.40 22.60

mfe-> 0 42 bo ■ ■ i ■■1 * 111 ■ 11.!!. । . I! ।. 1. 111,. ।. II11. M4 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 96.00 18.62% Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 22.00 22.20 22.40 22.60 54 m/z 191.00 17.88% 110 30 1 94 ■ i■111111 /1 ]. । ■ । 160 0 ■ " ■ 111'111 ■ ■11' " I " " r TIWWTIWWTTWWTTTUTTTTTTTTTTTTTT mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103348: Pyrazine, tetraethyl- (CAS) $$ tetraethyl pyrazine 192

177 22.00 22.20 22.40 22.60 5000 m/z 146.10 12.51%

53 67 - 81 149 163 i"'' i" " i "' ■ i" ■ ■ i ■"11 ■" ■ i ■" ■ i ■' ■' i 4m 0 11 1111 rnfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ............. 0.......... .. Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 22.00 22.20 22.40 22.60 m/z 193.00 11.97% A 5000

m/z—> 0 1100000011—000001* ■ | ■ H 139 15288 J 176

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 165 A 4 22.00 22.20 22.40 22.60

01140.D HP022102.M Tue Feb 26 08:30:18 2002 Page 14

NYC-WTC_000003520

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GCMS analysis results, sample AE01139, 2,4-DDD, Feb 2002 · Box DEP Box 12

NYC-WTC_000003483

Gas chromatography-mass spectrometry analysis report for sample AE01139 detecting surrogate 2,4-DDD at 76 ug with MDL of 5.0, analyzed on 02/27/2002.

1 shared topics · Same agency, volume and box · similarity 0.998