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GCMS analysis results for sample AE00613, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.

NYC-WTC_000051586–000051604

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN29\00613.D Vial: 2 • Acq On : 29 Jan 2002 3:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ****************************************************************** * * * Peak Number 10 N-perdeuteriobenzylideneani ... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 123610 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 50 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 Abundance Scan 1656 (22.280 min): 00613. D (-) m/z 192.10 100.00% 192

5000 ................. ............................

82 96 146 160 22.00 22.20 22.40 22.60 44 52 70 । | 118 mPTHTWTTTTT ................. ■i■ ' [rorrtT TTH m/z 191.10 19.19% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 ..... II..... A 22.00 22.20 22.40 22.60 54 m/z 146.10 16.07% 110 30 94 160 PPT " I " '11'' " I -HP " I" " I.......... . ■ ।|..................... . miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 . ...... A.... /I 22.00 22.20 22.40 22.60 5000 m/z 193.10 15.99%

96 139 152 165 176 8 .1, i' " 11 ■11 ■ i p 1 1' I I ■1" i ■1 ■ ■ i1" ' I1111111 + TTp m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102610: 2-Propenal, 3-(3,4-dimethoxyphenyl)- (CAS) $$ 3,4... 192 22.00 22.20 22.40 22.60 161 m/z 160.10 13.00%

5000

77 149 177 103 118 138 I mm M 4 64 89 ---P I 1’0’1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1 70 180 190 200 22.00 22.20 22.40 22.60

)0613.D SCAN508.M Wed Jan 30 09:02:09 2002 Page 12

NYC-WTC_000051601

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NYC-WTC_000051601Source: NYC Law Department, mirrored locally

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