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GCMS analysis results for sample AE00470, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00470 conducted on January 17, 2002.

NYC-WTC_000051697–000051713

Folder label: “GCMS X 1/9/02 A 1/15/02

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Scanned page image, NYC-WTC_000051711
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00470.D Vial: 4 Acq On : 15 Jan 2002 12:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 N-perdeuteriobenzylideneani ... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 80076 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual l N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 3 fluorene-9-spiro-cyclopropane 192 C15H12 000000-00-0 53 4 1,2-DI(3-THIENYL)ETHENE 192 C10H8S2 013640-84-1 53 Abundance Scan 1656 (22.280 min): 00470. D (-) m/z 192.10 100.00% 192

5000

■ ■ i ■ > ■ ■ i ■ ■ 96 146 160 i 22.00 22.20 22.40 22.60 44 70 82 0 —m ■ ।" ■ ■ । ■■ ■■ ।" " ।" n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 .. 'i... r........ i1 m/z 193.10 15.20% Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 22.00 22.20 22.40 22.60 54 110 m/z 191.10 14.70% 30 94 160 0 TTPTT '11" '11" " i "i1 Hmp " i ■ ■" i " ■' r " ' i ■" ' I' " ' i " ' ■ r ■ il TTp-.

/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 ■ • i ■ > • • i ■ • ■ ■ i ■ • » । i ■ i 22 00 22.20 22.40 22.60 5000 m/z 146.10 12.98%

9® 165 88 1 139 152 | 1/6 | 0 T1 " 11' ‘'11111'1 TUd ———uununnumnpWumgdknph T’T /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1 70 180 190 200 Abundance #103959: fluorene-9-spiro-cyclopropane 192 .. N...1 22.00 22.20 22.40 22.60 m/ z 96.00 12.70% 165 5000

n/z—> 0 4 1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 IPH 22.00 22.20 22.40 22.60

10470.D SCAN508.M Wed Jan 16 08:13:52 2002 Page 11

NYC-WTC_000051711

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NYC-WTC_000051711Source: NYC Law Department, mirrored locally

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