GCMS analysis results for sample AE03245, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.

NYC-WTC_000006085–000006104

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document L

Data File : C:\MSDCHEM\1\5973N\02MAR01\03245.D Vial: 6 • Acq On : 1 Mar 2002 2:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 N-perdeuteriobenzylideneani ... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 92936 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 3 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 46 4 fluorene-9-spiro-cyclopropane 192 C15H12 000000-00-0 42 Abundance Scan 1675 (22.283 min): 03245.D (-) m/z 192.00 100.00% 192

5000

96 146 160 82 49 0 TTIWTNTT 66 118 . .. ll,,,.. ■ i ■ ■ ■ f i ■ ■ ■ ■ । ■ ■ ■' ।1 f T-p-r TIT .... II 22.00 22.20 22.40 22.60 m/z 146.10 17.57% /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 ----- 22.00 22.20 22.40 22.60 54 110 m/z 191.10 17.28% 30 1 94 160 0 ""I.......... ■ ■ ।1 ■ • 11 ■ ■ ’ ■ 111111111 ■ । ■■■ TTPUUTTTTTTWWTIWWTTTWTTITTTTTT+ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192

22.00 22.20 22.40 22.60 5000 m/z 193.00 16.73%

m/z-> 0 88 J 96 165 139 152 ,| 176 1’1’111110011001110111010111111011111——0110100000110107111011001——3mrgnt 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 22.00 22.20 22.40 22.60 77 151 m/Z 96.00 15.64%

5000 93 104 130 I 119

m/z—> 0 TII I " ‘11" “ 1111111111111111 T‘1- 11’1 fn-r ‘ 1T ‘ I" " I " " I " " I " " I " ' I ' 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 177 mm , 22.00 22.20 22.40 22.60

)3245.D HP022102.M Mon Mar 04 12:33:07 2002 Page 15

NYC-WTC_000006103

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NYC-WTC_000006103Source: NYC Law Department, mirrored locally

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