GCMS analysis results for sample AE00844, Feb 26 2002

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Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052291–000052310

Folder label: “GCMS X 1/11/02 A 2/7/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00844.D vial : 7 Acq On : 7 Feb 2002 7:24 pm Operator: - Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 10 N-perdeuteriobenzylideneani ... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.13 ug/L 83612 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 2 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 49 3 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 45 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 45 Abundance Scan 1656 (22.280 min): 00844.D (-) m/z 192.10 100.00% 192

5000

82 96 146 160 22.00 22.20 22.40 22.60

m/z-> 0 44 ■ <11111 ■ I ■ IJ11 '. l * > < < । 120 TTTTT ‘ i ■ ■ ■ ■ ।. i ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 L m/z 191.10 17.83% Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 ■ । i 'i । ' 1 1 1 ' ’I1 22.00 22.20 22.40 22.60 54 m/z 146.10 15.58% 110 30 I 94 160 " i" ■ ■ i ■ mPH 0 , ITTHFTTT TTTTTT ' i " " r ■ " i " " i'1" b ' T /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine

77 130 151 192 ----- 22.00 22.20 22.40 22.60 L 93 104 m/z 193.10 14.76% 5000 119 1 177 0 " i ■ " ‘ i" 1' i " " i1 •'11 ■ ■ "i" ‘' i TTIT TTTT I’T -n-p- I TT 1'' I " " [ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102624:1 3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... 192 22.00 22.20 22.40 22.60 m/z 96.10 12.69%

5000

91 165 119 131 0 " । ■ ■' ■ । ■1'1111' ■ ।1' ■ ■ ।।■ 1 ■ ■ 11 " '' I"J | 103 __ JI 147 I 11177 " I " " I" " I' " ' I"'' I '1'' I " ' * I " " r TII n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

00844.D HP020702.M Thu Feb 21 09:58:17 2002 Page 12

NYC-WTC_000052306

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NYC-WTC_000052306Source: NYC Law Department, mirrored locally

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