GCMS analysis results for sample AE00844, Feb 26 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052291–000052310

Folder label: “GCMS X 1/11/02 A 2/7/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00844.D Vial: 7 Acq On : 7 Feb 2002 7:24 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Methane, bromo- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 13.37 0.06 ug/L 32083 Naphthalene-d8 13.19 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromo- 94 CH3Br 000074-83-9 4 2 2-Methyl-3-methoxy-4H-pyran-4-one 140 C7H8O3 000000-00-0 4 3 Cyclohexanepropanol, 2-acetoxy- 200 C11H20O3 000000-00-0 4 4 n-C5HHC (CH3) =C (CH3) 2 $$ 2,3-Dim. . . 140 C10H20 019781-18-1 3 Abundance Scan 876 (13.375 min): 00844.D (-) m/z 140.10 100.00% 14,0

5000

68 94 13.00 13.20 13.40 13.60 13.80 84 || 0 ■ > i ■' ■ ■ i ■ ■ ■ ■ i' ■ ■' i ■ ■'' i' ■' ■ i ■1 ■ ■ ■ ■ i'' ■' i ‘■ i ■' ■ ■ i'' ■' i''' ■ 11 b m/ z 94.10 13.83% m/z-> 10 20 30 40 50 601 70 80 90 100 110 120 130 140 150 160 Abundance ;#5692: Methane, bromo- 15 94

m ri । । , 5000 13.00 13.20 13.40 13,60 13.80 m/z 68.10 11.06%

mfe-> Abundance 0 20 47 >■.... .... । > ■ > ■ । ■ > ■ 11 ■ 30 40 50 60 70 a 79

80 ■ i ■ ■ ■ • i i ■ ■ ■ ■ i 90 100 110 120 130 140 150 160 #35380: 2-Methyl-3-methoxy-4H-pyran-4-one ‘II

69 140 122 .... r... ...... 13.00 13.20 13.40 13.60 13.80 5000 m/ z 96.10 9.08%

82 110 97 o1 ...................... Il1.... || T’t’t I ’ ’ || i ■'1' i Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #115091: Cyclohexanepropanol, 2-acetoxy- ■ । 1 ■ 1 ■ i ■ 1 ■ ■ i ■1 ■ 1 । 1 43 13.00 13.20 13.40 13.60 13.80 m/z 70.10 8.65% 5000 67 94 79

0 " i11" i1" 11"1111 " i" " i111 1111' ।11 r 1 1107122. 140. 158 1 ' T' ' 1 1 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 13.00 13.20 13.40 13.60 13.80

00844.D HP020702.M Thu Feb 21 09:58:17 2002 Page 11

NYC-WTC_000052305

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000052305Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis results for sample AE00842, Feb 2002 · Box DEP Box 28

NYC-WTC_000052251

Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.

1 shared topics · Same agency, volume and box · similarity 0.999