GCMS analysis results for sample AE08960, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08960 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049571–000049583

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

•Data File : C:\MSDCHEM\1\DATA\020424\08960.D Vial: 11 Acq On : 24 Apr 2002 7:42 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Methane, bromodichloro Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.35 0.23 ug/1 288818 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 78 2 Methane, bromodichloro- 162 CHBrC12 000075-27-4 78 3 Methane, bromodichloro- 162 CHBrC12 000075-27-4 74 4 Methane, bromodichioro- 162 CHBrC12 000075-27-4 72 Abundance Scan 46 (3.350 min): 08960.D (-36) (-) m/z 82.95 100.00% 80 40

5000

127 Amm 7! Mnm q m , M . 3.20 3.30 3.40 3.50 3.60 3.70 3.80 rl‘‘211‘Tt1233 ,ll 121 '11 “ “ I • ■ " I ‘ II, ‘ I ‘‘ I ■ ■ ‘' I' ■ ’ I’ ■'' I''' ‘ I ‘‘ ■ I ‘' I'' m/z 40.10 70.00% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33236: Methane, bromodichloro- 83

5000 ‘ 3.20 3.30 3.40 3.50 3.60 3.70 3.80 47 m/z 85.00 66.80% „ 129 miz-> .13127,235 ....1163..72.. 123.100...110116, 10 20 30 40 50 60 70 80 7..,..... 194.1 120 130 140 150 160 170 Abundance #116497: Methane, bromodichloro- 83 A. 1M? Man APAMMA 3.20 3.30 3.40 3.50 3.60 3.70 3.80 5000 m/z 47.10 22.97%

iz-> Abundance .. ... 227,.%........ 1,1.1. 191— ...... 11129....... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #116496: Methane, bromodichloro- udl nuppau 80 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/z 48.10 19.31% 5000

,,, 2r 47

........’ 1.158 70 ............. 1111—000 10mnmnmunmammmummeTnTT 116... .............. . 123 Mywoo/ MeOok ■*■। । । ■111111 11 “ i ■"111 ■ iz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.20 3.30 3.40 3.50 3.60 3.70 3.80

08960.D SCAN020424.M Thu May 02 14:44:20 2002 Page 3

NYC-WTC_000049577

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GCMS analysis results for sample AE08964, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049622

Laboratory report documenting GCMS analysis of sample AE08964 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998