GCMS analysis results for sample AE08960, May 7, 2002

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Data File : C:\MSDCHEM\l\DATA\020424\08960 .D Vial: 11 Acq On : 24 Apr 2002 7:42 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Acetonitrile, dichloro- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 3.65 0.24 ug/1 297711 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 72 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 3 Chloral Hydrate 164 C2H3C1302 000302-17-0 43 4 Acetaldehyde, trichloro- 146 C2HC130 000075-87-6 43 Abundance Scan 97 (3.649 min): 08960.D (-93) (-) m/z 74.05 100.00% 74

5000 47 ------ 3.40 3.60 3.80 4.00 1 374 T 'l. . |.... 1. <. 11......... |.... |... 1111111.1 U 11111111111.11111111111 n 1111'. 11 m/z 81.95 65.14% m/z—> 0 20 40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 360 Abundance #28338: Acetonitrile, dichloro- 74

5000 47 _A 3.40 3.60 3.80 4.00 rn/z 84.00 39.59% , 108 miz-> Abundance o T 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 380 " #115342: Acetonitrile, dichloro- w"pw Wonowaw 74 35 1 1 i ■ 1 1 ■ i ■ ■ ' ■ i ■ ■ ■ ■ i ■ • 3.40 3.60 3.80 4.00 5000 rn/z 76.00 31.95%

miz—> mm T ... 11... I.I....t,... 1.111!11111111111111!11111111111111111111111111 0 20 40 60 80 100120140160180 200220240 260 280 300320 340 360 Abundance 82 #116338: Chloral Hydrate , L.... .A___ Ti J » : » ’It I » ’I 1 I I J I I I 3.40 3.60 3.80 4.00 m/z 47.05 _______ 26.05% 5000 29 47

ml.65 ............. . 111 wAput tnfz~> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360’ ■ ‘ i ■ 1 1 • i ' 1 1 ' i 1 1 1 ■ i 1 ' 3.40 3.60 3.80 4.00

08960.D SCAN020424.M Thu May 02 14:44:22 2002 Page 4

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