GCMS analysis results for sample AE08970, May 7, 2002

NYC 9/11 Public Portal Document

’Data File : C:\MSDCHEM\1\DATA\020424\08970.D Vial: 18 Acq On : 25 Apr 2002 2:34 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Acetonitrile, dichloro­ Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 3.65 0.20 ug/1 242045 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 3 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 9 4 Propanoic acid. 74 C3H602 000079-09-4 5 Abundance Scan 98 (3.655 min): 08970.D (-92) (-) m/z 74.00 100.00% 74

82 5000 40 47 -. * P ioh", 3.40 3.60 3.80 4.00

miz-> —TTT 10 20 30 HHl 40 — 60 50 •1**1* i 1 70 80 • i ■ ■ • 1 1 1 1 • • i ‘ 90 100 110 • 1 i m/z 82.00 50.69% Abundance #28338: Acetonitrile, dichloro- 74 ------- 5000 82 3.40 3.60 3.80 4.00 47 35 m/z 40.10 38.09% 12 Pm! .2.,. 1,1.'. 621 1 1 I 1 1 1 1 1 1 TI . 108 ■ • i ■ ■ • 1 i 1 • ' 1 I ■ ‘ • i miz-> 10 201 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 1 ■1 • । ■ • ■ ■ । ‘111 •111111' 3.40 3.60 3.80 4.00 5000- 82 m/z 84.00 36.00% 47 "ArMWw • .-f । । । ' I ' * 1 — ■ i ■ ■ • ■ i ■ 11444/11 4 1 1 I I m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28312:3,3-Dichloropropyne ■ ■ ‘ ■ i • ■ • 1 i • • ‘ ‘ "I 1 1 1 1 I 1 1 1 TH 3.40 3.60 3.80 4.00 m/z 76.00 32.90% 5000- 38 47 1 i 53 60 m/z—> ..10p20 . 28, 30 . 'll 401 ‘ 1 11 501 1*1111 60 70 82 1 i • ■ ‘ • i 1 1 1 ri 1 80 90 100 108 110 • । ‘ । 11 i ’ >11111 1 3.40 3.60 A, , i pP i r 3.80 4.00

08970.D SCAN020424.M Thu May 02 15:01:18 2002 Page 4

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