GCMS analysis results for sample AE08969, May 7, 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\020424\08969.D Vial: 17 Acq On : 25 Apr 2002 1:35 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Acetonitrile, dichloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.65 0.31 ug/1 371244 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 9 2 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 4 3 Boron trifluoride etherate 142 C4H10BF3O 000109-63-7 4 4 Allyl mercaptan 74 C3H6S 000870-23-5 3 Abundance Scan 98 (3.655 min): 08969.D (-93) (-) m/z 74.10 100.00% 74 82 5000 47 ' I ■ " 35 58 3.40 3.60 3.80 4.00

iz-> 110........ podplyotilpo 20 30 40 50 — 1111 । ‘It ■1 i1 ■ ‘ ■ I ■1 1 ‘ i ■ '1 ■ i' ‘ ■11 ■' m/z __ 82.00 60.57% 60 70 80 90 100 110 120 130 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 3.40 3.60 3.80 4.00 47 m/z 84.00 41.54%

miz-> Abundance * i • * • * i • 10 20 TT upas TTyT-rr-rp- 30 40 50 60 70 80 90 #28312: 3,3-Dichloropropyne 1 ‘.i ■ ■ ‘ ■ i • ■ • • i ‘ 100 110 120 130 ' i ■ ■ ■41 • ■

WPP/Wz 74 11 ■ ■ । •1 ■ ■ i • ‘ • i1 ■1111 ■' 3.40 3.60 3.80 4.00 5000 m/z 76.00 38.61% 38 47

miz->10 ......20 2.11,., I, 53 60 1' I'71 ■ i' ■ " I 30 40 50 60 70 80 90 100 110 120 130 82 ‘1110110211055—1333131 108 ..... ................ Abundance #1099: Boron trifluoride etherate -r-r-pn-n-y 31 3.40 3.60 3.80 4.00 m/z 47.05 24.02% 59 5000 45 74 Miojwo4 miz—> - 10 15 20 all30+3944 — 66 40 50 60 70 80 90 100 , .81 93 !' ■ t f1 ‘1 i1 **14**14* 110 120 127 130 ■11 • ■ ■ • i ■■■ ■ ■ ■ i ■ * ■ ■ i ■1 3.40 3.60 3.80 4.00

08969.D SCAN020424.M Thu May 02 15:00:33 2002 Page 4

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